Syntheses, crystal structures and properties of tetra-kis-(3-methyl-pyridine-κ N)bis-(iso-thio-cyanato-κ N)manganese(II) and tetra-kis-(3-methyl-pyridine-κ N)bis-(iso-thio-cyanato-κ N)iron(II) [0.03%]
四(3-甲基吡啶-N)-双(异硫氰酸根合-N)锰(II)和四(3-甲基吡啶-N)-双(异硫氰酸根合-N)铁(II)的合成、晶体结构和性质研究
Magdalena Ceglarska,Christoph Krebs,Christian Näther
Magdalena Ceglarska
The reaction of Mn(NCS)2 or Fe(NCS)2 with 3-methyl-pyridine (C6H7N) leads to the formation of two isostructural compounds with compositions [Mn(NCS)2(C6H7N)4] (1) and [Fe(NCS)2(C6H7N)4] (2). IR spectroscopic investigations indicate that onl...
Synthesis and crystal structure of rac-2-(1,3-dioxo-isoindolin-2-yl)ethyl 4-methyl- N-phenyl- N'-(tri-iso-propyl-sil-yl)benzene-sulfondiimidoate: the first member of a new substance class [0.03%]
外消旋体-2-(1,3-二氧代异靛红-2-基)乙基 4-甲基-N-苯基-N'-(三异丙基硅基)苯磺酰双亚胺酯的合成及其晶体结构：一种新物质类别的首例成员
Erik Friedrich,Timo Heinrich,Lara Rosenberger et al.
Erik Friedrich et al.
The title compound {systematic name: rac-2-[7-methyl-4-(4-methylphenyl)-4-(phenylimino)-6,6-bis(propan-2-yl)-3-oxa-4λ6-thia-5-aza-6-silaoct-4-en-1-yl]-2,3-dihydro-1H-isoindole-1,3-dione}, C32H41N3O3SSi, was synthesized by desoxychlorinatio...
Crystal structures of methyl 3,5-di-methyl-benzoate, 3,5-bis-(bromo-meth-yl)phenyl acetate and 5-hy-droxy-benzene-1,3-dicarbaldehyde [0.03%]
3,5-二甲基苯甲酸甲酯、3,5-双(溴甲基)苯乙酸酯和5-羟基苯-1,3-二甲醛的晶体结构
Ben Ebersbach,Wilhelm Seichter,Monika Mazik
Ben Ebersbach
The crystal structures of the title compounds, methyl 3,5-di-methyl-benzoate (C10H12O2; 1), 3,5-bis-(bromo-meth-yl)phenyl acetate (C10H10Br2O2; 2) and 5-hy-droxy-benzene-1,3-dicarbaldehyde (C8H6O3; 3) were determined by single-crystal X-ray...
Crystal structures of three zinc(II) halide coordination complexes with quinoline N-oxide [0.03%]
含喹啉-N-氧化物的三种锌(II)卤化物配位化合物的晶体结构
Clifford W Padgett,Will E Lynch,Erin N Groneck et al.
Clifford W Padgett et al.
The reaction of one equivalent of zinc(II) halide with two equivalents of quinoline N-oxide (QNO) in methanol yields compounds as ZnX 2(QNO)2, where X = Cl (I), Br (II) and I (III), namely, di-chlorido-bis-(quinoline N-oxide-κO)zinc(II), [...
Crystal structure and Hirshfeld surface analysis of 2-chloro- N-(4-meth-oxy-phen-yl)acetamide [0.03%]
2-氯-N-(4-甲氧基苯基)乙酰胺的晶体结构和Hirshfeld面分析
Mohcine Missioui,Walid Guerrab,Intissar Nchioua et al.
Mohcine Missioui et al.
In the title mol-ecule, C9H10ClNO2, the meth-oxy group lies very close to the plane of the phenyl ring while the acetamido group is twisted out of this plane by 28.87 (5)°. In the crystal, a three-dimensional structure is generated by N-H...
Synthesis and crystal structure of [(Sp )-(2-phenyl-ferrocen-yl)meth-yl]tri-methyl-ammonium iodide di-chloro-methane monosolvate [0.03%]
(S+)-2-苯基环己二烯基甲基)三甲基铵碘化物 dichloromethane溶剂化物的合成和晶体结构
Abdelhak Lachguar,Eric Deydier,Agnès Labande et al.
Abdelhak Lachguar et al.
As a follow-up to our research on the chemistry of disubstituted ferrocene derivatives, the synthesis and the structure of the title compound, [Fe(C5H5)(C15H19N)]I·CH2Cl2, is described. The cation mol-ecule is built up from a ferrocene dis...
Flux syntheses and single-crystal structures of CsNa10 M 4(AsO4)9 (M = Zr, Hf) [0.03%]
CsNa10M4(AsO4)9(M=Zr,Hf)的合成及单晶结构研究
William T A Harrison
William T A Harrison
The isostructural compounds caesium deca-sodium tetra-zirconium nona-arsenate, CsNa10Zr4(AsO4)9, and caesium deca-sodium tetra-hafnium nona-arsenate, CsNa10Hf4(AsO4)9, arose as unexpected single-crystal products from the reactions of Na2CO3...
Crystal structure and Hirshfeld surface analysis of (E)-2-(4-bromo-phen-yl)-1-[2,2-di-bromo-1-(4-nitro-phen-yl)ethen-yl]diazene [0.03%]
(E)-2-(4-溴苯基)-1-[2,2-二溴-1-(4-硝基苯基)乙烯基]叠氮的晶体结构和Hirshfeld面分析
Mehmet Akkurt,Sema Öztürk Yıldırım,Namiq Q Shikhaliyev et al.
Mehmet Akkurt et al.
The mol-ecule of the title compound, C14H8Br3N3O2, consists of three almost planar groups: the central di-bromo-ethenyldiazene fragment and two attached aromatic rings. The mean planes of these rings form dihedral angles with the plane of t...
Crystal structure and Hirshfeld surface analysis of 2,2'-(phenyl-aza-nedi-yl)bis-(1-phenyl-ethan-1-one) [0.03%]
2,2'-（苯基氮烯二基）双（1-苯乙酮）的晶体结构和Hirshfeld面分析
Farid N Naghiyev,Victor N Khrustalev,Marina G Safronenko et al.
Farid N Naghiyev et al.
The whole mol-ecule of the title compound, C22H19NO2, is generated by twofold rotational symmetry. The N atom exhibits a trigonal-planar geometry and is located on the twofold rotation axis. In the crystal, mol-ecules are linked by C-H⋯O c...
Halogen-bonded zigzag mol-ecular network based upon 1,2-di-iodo-perchloro-benzene and the photoproduct rctt-1,3-bis-(pyridin-4-yl)-2,4-di-phenyl-cyclo-butane [0.03%]
基于1,2-二碘四氯苯和光产物rctt-1,3-双(吡啶-4-基)-2,4-二苯基环丁烷的卤素键正交分子网络
Taylor J Dunning,Eric Bosch,Ryan H Groeneman
Taylor J Dunning
The formation and crystal structure of a zigzag mol-ecular network held together by I⋯N halogen bonds is reported. In particular, the halogen-bond donor is 1,2-di-iodo-perchloro-benzene (1,2-C6I2Cl4 ) while the acceptor is a head-to-tail p...