Synthesis, crystal structure and Hirshfeld surface analysis of a zinc(II) coordination polymer of 5-phenyl-1,3,4-oxa-diazole-2-thiol-ate [0.03%]
5-苯基-1,3,4-氧氮杂茂-2-硫代
Mehribon Pirimova,Batirbay Torambetov,Shakhnoza Kadirova et al.
Mehribon Pirimova et al.
A new zinc coordination polymer with 5-phenyl-1,3,4-oxa-diazole-2-thiol-ate, namely, catena-poly[zinc(II)-bis-(μ2-5-phenyl-1,3,4-oxa-diazole-2-thiol-ato)-κ2 N 3:S;κ2 S:N 3], [Zn(C8H5N2OS)2] n , was synthesized. The single-crystal X-ray d...
Crystal structure of the complex of 2,4,6-tri-ethyl-1,3,5-tris-[(4-methyl-1 H-indazol-1-yl)meth-yl]-benzene with NH4PF6 [0.03%]
含NH4PF6的2,4,6-三乙基-1,3,5-三[（4-甲基-1H-吲达唑-1-基）甲基]苯的晶体结构
Felix Fuhrmann,Eric Meier,Wilhelm Seichter et al.
Felix Fuhrmann et al.
The complex of 2,4,6-tri-ethyl-1,3,5-tris-[(4-methyl-1H-indazol-1-yl)meth-yl]-benz-ene with ammonium hexa-fluorophosphate, C39H42N6·NH4 +·PF6 -, crystallizes in the monoclinic space group P21 with two mol-ecules of the receptor, two NH4 +...
Synthesis and crystal structure of hydrated μ-oxa-lato-bis-{bis-[3-methyl-5-(pyridin-2-yl)-1 H-1,2,4-triazole]iron(II)} bis-(toluene-sulfonate) 2.75-hydrate [0.03%]
含水μ-氧桥联双-{双[3-甲基-5-(吡啶-2-基)-1H-1,2,4-三氮唑]铁(II)}双-(对甲苯磺酸盐)配合物的合成和晶体结构
Yuliia P Petrenko,Yurii S Bibik,Dmytro M Khomenko et al.
Yuliia P Petrenko et al.
In the title compound [Fe2(C2O4)(C8H8N4)4](CH3C6H4SO3)2·2.75H2O, the two FeII ions have a highly distorted octa-hedral FeN4O2 environment formed by two bidentate triazole-based chelating ligands and a bis-bidentate oxalate bridging anion t...
Syntheses and crystal structures of a nitro-anthracene-isoxazole and its oxidation product [0.03%]
硝基蒽异唑及其氧化产物的合成与晶体结构测定
Chun Li,Matthew J Weaver,Michael J Campbell et al.
Chun Li et al.
The syntheses and structures of an unexpected by-product from an iodination reaction, namely, ethyl 5-methyl-3-(10-nitro-anthracen-9-yl)isoxazole-4-carb-oxy-l-ate, C21H16N2O5, (I), and its oxidation product, ethyl 3-(9-hy-droxy-10-oxo-9,10-...
Crystal structure and Hirshfeld surface analysis of 4-bromo-2-[3-methyl-5-(2,4,6-tri-methyl-benz-yl)oxazolidin-2-yl]phenol [0.03%]
4-溴-2-[3-甲基-5-(2,4,6-三甲基苯基)氧氮杂环丁-2-基]酚的晶体结构和Hirshfeld面分析
Ali N Khalilov,Victor N Khrustalev,Elena A Fortalnova et al.
Ali N Khalilov et al.
The title compound, C20H24BrNO2, is chiral at the carbon atoms on either side of the oxygen atom of the oxazolidine ring and crystallizes as a racemate. The 1,3-oxazolidine ring adopts an envelope conformation with the N atom in an endo pos...
Crystal growth, structure elucidation and CHARDI/BVS investigations of β-KCoFe(PO4)2 [0.03%]
β-KCoFe(PO4)2的晶体生长、结构解析及CHARDI/BVS研究
Adam Bouraima,Said Ouaatta,Jamal Khmiyas et al.
Adam Bouraima et al.
Single crystals of β-KCoFe(PO4)2, potassium cobalt(II) iron(III) bis-(ortho-phosphate), were grown from the melt under atmospheric conditions. This phosphate crystallizes isotypically with KZnFe(PO4)2 in space group C2/c, adopting a zeolit...
Volker Kahlenberg
Volker Kahlenberg
Single crystals of (K1.52Na0.48)Ca3Si3O10 [idealized (K1.5Na0.5)Ca3Si3O10, di(pot-assium, sodium) tricalcium tris-ilicate], were obtained from the crystallization of a glass with a molar oxide ratio of K2O:Na2O:CaO:SiO2 = 1.5:0.5:6:6 that w...
Crystal-structure studies of 4-phenyl-piperazin-1-ium 4-eth-oxy-benzoate monohydrate, 4-phenyl-piperazin-1-ium 4-meth-oxy-benzoate monohydrate, 4-phenyl-piperazin-1-ium 4-methyl-benzoate monohydrate and 4-phenyl-piperazin-1-ium tri-fluoro-acetate 0.12-hydrate [0.03%]
4-苯基哌嗪鎓-4-乙氧基苯甲酸单水合物，4-苯基哌嗪鎓-4-甲氧基苯甲酸单水合物，4-苯基哌嗪鎓-4-甲基苯甲酸单水合物和4-苯基哌嗪鎓三氟乙酸0.12水合物的晶体结构研究
Ninganayaka Mahesha,Haruvegowda Kiran Kumar,Mehmet Akkurt et al.
Ninganayaka Mahesha et al.
In this study, four new piperazinium salts, namely, 4-phenyl-piperazin-1-ium 4-eth-oxy-benzoate monohydrate, C9H9O3·C10H15N2·H2O (I); 4-phenyl-piperazin-1-ium 4-meth-oxy-benzoate monohydrate, C10H15N2·C8H7O3·H2O (II); 4-phenyl-piperazin...
Synthesis and crystal structure of 2-(2-hy-droxy-phen-yl)-1,3-bis-(4-meth-oxy-benz-yl)-1,3-diazinan-5-ol [0.03%]
2-(2-羟基苯基)-1,3-双(4-甲氧基苯基)吗啉
Augusto Rivera,Jaime Ríos-Motta,Michael Bolte
Augusto Rivera
The redetermined structure of 2-(2-hy-droxy-phen-yl)-1,3-bis-(4-meth-oxy-benz-yl)-1,3-diazinan-5-ol, C26H30N2O4, at 173 K has ortho-rhom-bic (Pbca) symmetry. It was previously described by Bolte et al. [ Private Communication (refcode EWICE...
Synthesis and crystal structure of bis-[ trans-di-aqua-(1,4,8,11-tetra-aza-cyclo-tetra-decane-κ4 N 1, N 4, N 8, N 11)nickel(II)] trans-(1,4,8,11-tetra-aza-cyclo-tetra-decane-κ4 N 1, N 4, N 8, N 11)bis-[4,4',4''-(1,3,5-tri-methyl-benzene-2,4,6-tri-yl)tris-(hydrogen phenyl-phospho-nato-κ O)]nickel(II) deca-hydrate [0.03%]
合成了一个Ni-II化合物并研究了其晶体结构：双-[四-(1,4,8,11-四氮杂环十四烷-基)均-四水合镍(II)] 双-[4,4', 4''-(1,3,5-三甲基苯-2,4,6-三基)-三(氢苯基磷酸酯ato-O)] 均Ni(II)十水合物
Liudmyla V Tsymbal,Rodinel Ardeleanu,Sergiu Shova et al.
Liudmyla V Tsymbal et al.
The components of the title compound, [Ni(C10H24N4)(H2O)2]2[Ni(C10H24N4)(C27H24O9P3)2]·10H2O are two centrosymmetric [Ni(C10H24N4)(H2O)2]2+ dications, a centrosymmetric [Ni(C10H24N4)(C27H24O9P3)2]4- tetra-anion and five crystallographicall...