Synthesis, crystal structure and Hirshfeld surface analysis of aqua-(3-meth-oxy-cinnamato-κ O)bis-(1,10-phenanthroline-κ2 N, N')cobalt(II) nitrate [0.03%]
硝酸二(1,10-菲罗啉)(3-甲氧基肉桂酸根)钴(II)水合物的合成，晶体结构和 Hirshfeld 表面分析
Asma Lehleh,Mehdi Boutebdja,Chahrazed Beghidja et al.
Asma Lehleh et al.
The title compound, [Co(C10H9O3)(C12H8N2)2(H2O)]NO3 (I), crystallizes in the triclinic space group P with a monomeric [Co(3-meo-cin)(phen)2(H2O)]+ cation and a nitrate anion (3-meo-cin = 3-meth-oxy cinnamic acid) in the asymmetric unit. The...
Crystal structure of bis-{3-(3-bromo-4-methoxyphenyl)-5-[6-(1 H-pyrazol-1-yl)pyridin-2-yl]-1,2,4-triazol-3-ato}-iron(II) methano-l disolvate [0.03%]
双[3-(3-溴-4-甲氧基苯基)-5-[6-(1H-吡唑-1-基)吡啶-2-基]-1,2,4-三唑-3-基]铁(II)甲醇二溶剂的晶体结构
Kateryna Znovjyak,Igor O Fritsky,Tatiana Y Sliva et al.
Kateryna Znovjyak et al.
The unit cell of the title compound, [FeII(C17H12BrN6O)2]·2MeOH, consists of a charge-neutral complex mol-ecule and two independent mol-ecules of methanol. In the complex mol-ecule, the two tridentate ligand mol-ecules 2-[5-(3-bromo-4-meth...
Syntheses and structural characterizations of the first coordination polymers assembled from the Ni(cyclam)2+ cation and the benzene-1,3,5-tri-carboxyl-ate linker [0.03%]
首例由Ni(cyclam)2+阳离子和苯-1,3,5-三羧酸配体组装的配位聚合物的合成及结构表征
Sergey P Gavrish,Sergiu Shova,Yaroslaw D Lampeka
Sergey P Gavrish
The asymmetric unit of catena-poly[[[(1,4,8,11-tetra-aza-cyclo-tetra-decane-κ4 N 1,N 4,N 8,N 11)nickel(II)]-μ2-5-carb-oxy-benzene-1,3-di-carboxyl-ato-κ2 O 1:O 3] octa-hydrate], {[Ni(C9H4O6)(C10H24N4)]·8H2O} n (I), consists of a macrocyc...
Synthesis and crystal structure of 2-(1,3-dithietan-2-yl-idene)cyclo-hexane-1,3-dione [0.03%]
2-(1,3-二硫杂环丁烷-2-亚基)环己烷-1,3-二酮的合成及晶体结构分析
Sabah Kellou,Ouarda Brihi,Souheyla Chetioui et al.
Sabah Kellou et al.
The title compound, C8H8O2S2, contains a cyclo-hexane-1,3-dione ring, which has a twist-boat conformation. The C2S2 ring is close to planar (r.m.s. deviation = 0.023 Å) and the dihedral angle between the mean planes of the cyclo-hexane and...
Synthesis and crystal structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone [0.03%]
2-氯-1-(3-羟基苯基)乙酮的合成及其晶体结构分析
Prabhakar Priyanka,Bidarur K Jayanna,Vinaya et al.
Prabhakar Priyanka et al.
The structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone, C8H7ClO2, an α-halo-ketone is described. The mol-ecule is planar (r.m.s. deviation = 0.0164 Å) and in the crystal, inversion-symmetric dimers are formed as a result of pairs of str...
Chandru P Chandrasekaran,James P Donahue
Chandru P Chandrasekaran
The planar title compound 4,5-dimethyl-1,3-dioxol-2-one, C5H6O3, 1, crystallizes with its mol-ecular C 2 axis coincident with a crystallographic mirror plane in space group P21/m. In the plane defined by the b axis and an ac face diagonal, ...
Synthesis, crystal structure and properties of catena-poly[[[bis-(3-methyl-pyridine-κ N)nickel(II)]-di-μ-1,3-thio-cyanato] aceto-nitrile monosolvate] [0.03%]
聚[[双(3-甲基吡啶-N)镍(II)]二-μ-1,3-硫氰酸盐]丙腈单溶剂合物的合成、晶体结构及性质
Christian Näther,Inke Jess,Christoph Krebs
Christian Näther
In the crystal structure of the title compound, {[Ni(NCS)2(C6H7N)2]·CH3CN} n , the NiII cation is octa-hedrally coordinated by two N-bonding and two S-bonding thio-cyanate anions, as well as two 3-methyl-pyridine coligands, with the thio-c...
Synthesis, crystal structures, and Hirshfeld analysis of three hexa-hydro-quinoline derivatives [0.03%]
三种六氢喹啉衍生物的合成、晶体结构及Hirshfeld表征分析
Scott A Steiger,Chun Li,Allen G Oliver et al.
Scott A Steiger et al.
Three hexa-hydro-quinoline derivatives were synthesized and crystallized in an effort to study the structure-activity relationships of these calcium-channel antagonists. The derivatives are ethyl 4-(2-meth-oxy-phen-yl)-2,7,7-trimethyl-5-oxo...
Tri-methyl-pyrazole: a simple heterocycle reflecting Kitaigorodskii's packing principle [0.03%]
三甲基吡唑：一个简单的杂环体现Kitaigorodskii的堆积原则
Steven van Terwingen,Ulli Englert
Steven van Terwingen
The five-membered heterocycle 1,3,5-trimethyl-1H-pyrazole, C6H10N2 (1) crystallizes in space group Pnma with all non-hydrogen atoms of the mol-ecule on the crystallographic mirror plane. This arrangement has been recognized as favorable wit...
Crystal structure of chlorido-[diphen-yl(thio-phen-2-yl)phosphine-κ P]gold(I) [0.03%]
氯化双(二苯基(硫亚苯基)磷烷-κP)金(I)的晶体结构
Thomas Neils,Andrew LaDuca,John E Bender et al.
Thomas Neils et al.
The crystal structure of the title compound, [AuCl(C16H13PS)], is reported. The mol-ecular structure features a nearly linear arrangement of the chloride and phosphino ligands around the gold(I) center, with a P-Au-Cl bond angle of 179.42 (...