Synthesis, crystal structure and Hirshfeld surface analysis of bis-(caffeinium) hexa-chlorido-platinum(IV) in comparison with some related compounds [0.03%]
双咖啡因六氯铂(IV)的合成、晶体结构及Hirshfeld表面分析与其一些相关化合物的比较研究
Karim A Zagidullin,Anton P Novikov,Daria A Zelenina et al.
Karim A Zagidullin et al.
The mol-ecular and crystal structure of the title compound, (C8H11N4O2)2[PtCl6], synthesized from hexa-chloro-platinic acid and caffeine in methanol, was studied by single-crystal X-ray diffraction. The caffeinium cations form a double laye...
catena-Poly[[bis-(di-aqua-lithium)]-μ4-3,3',5,5'-tetra-nitro-4,4'-bi-pyrazole-1,1'-diido]: a new moisture-insensitive alkali-metal energetic salt with a well-defined network structure [0.03%]
新型含水合碱金属的低感湿性硝酸酯类盐化合物catena-聚[[双(二水合锂)]-4,4'-联吡唑-3,3',5,5'-四硝酸根]：独特的网络结构及其性能研究
Kostiantyn V Domasevitch,Ganna A Senchyk,Harald Krautscheid
Kostiantyn V Domasevitch
In the structure of the title salt, [Li2(C6N8O8)(H2O)4]n, the 3,3',5,5'-tetra-nitro-4,4'-bi-pyrazole-1,1'-diide dianion [{TNBPz}2-] is situated across the twofold axis. The distorted coordination octa-hedra around Li+ involve four short bon...
Crystallographic and spectroscopic characterization of two 1-phenyl-1 H-imidazoles: 4-(1 H-imidazol-1-yl)benzaldehyde and 1-(4-meth-oxy-phen-yl)-1 H-imidazole [0.03%]
两个1-苯基-1H-咪唑的晶体学和光谱表征：4-（1H-咪唑-1-基）苯甲醛和1-（4-甲氧基苯基）-1H-咪唑
Isobelle F McClements,Clara R Wiesler,Joseph M Tanski
Isobelle F McClements
The title compounds, C10H8N2O, (I), and C10H10N2O, (II), are two 1-phenyl-1H-imidazole derivatives, which differ in the substituent para to the imidazole group on the arene ring, i.e. a benzaldehyde, (I), and an anisole, (II). Both mol-ecul...
Structure of (R, R)-4-bromo-2-{4-[4-bromo-1-(4-toluene-sulfon-yl)-1 H-pyrrol-2-yl]-1,3-di-nitro-butan-2-yl}-1-(4-toluene-sulfon-yl)-1 H-pyrrole, another ostensible by-product in the synthesis of geminal-dimethyl hydro-dipyrrins [0.03%]
(R,R)-4-溴-2-{4-[4-溴-1-(对甲苯磺酰基)-1H-吡咯-2-基]-1,3-二硝基丁-2-基}-1-(对甲苯磺酰基)-1H-吡咯的结构，双甲基双吡咯烷合成中另一种假想副产物
Harry C Sample,Brendan Twamley,Mathias O Senge
Harry C Sample
The crystal structure of (R,R)-4-bromo-2-{4-[4-bromo-1-(4-toluene-sulfon-yl)-1H-pyrrol-2-yl]-1,3-di-nitro-butan-2-yl}-1-(4-toluene-sulfon-yl)-1H-pyrrole (1, C26H24Br2N4O8S2) is presented. The title compound was isolated in suitable yield as...
Kambarali K Turgunov,Ulli Englert
Kambarali K Turgunov
Three coordination compounds of quinazolin-4(3H)-one (quinoz; C8H6N2O) with divalent group 12 halides are reported. In all complexes, coordination occurs via the nitro-gen atom ortho to the quinazolinone carbonyl group. In the two chain pol...
Crystal structure and Hirshfeld surface analysis of (1 H-imidazole-κ N3)[ N-(2-oxido-benzyl-idene)tyrosinato-κ3O, N, O']copper(II) [0.03%]
(1H-咪唑-κN3)[N-(2-氧化苯甲酰)酪氨ato-κ3O,N,O′]合铜(II)的晶体结构和Hirshfeld面分析
Soma Suzuki,Yukihito Akiyama,Daisuke Nakane et al.
Soma Suzuki et al.
The title copper(II) complex, [Cu(C16H13NO4)(C3H4N2)], consists of a tridentate ligand synthesized from l-tyrosine and salicyl-aldehyde. One imidazole mol-ecule is additionally coordinating to the copper(II) ion. The crystal structure featu...
Cyclo-penta-dienone triisocyanide iron complexes: general synthesis and crystal structures of tris-(2,6-di-methyl-phenyl isocyanide)(η4-tetra-phenyl-cyclo-penta-dienone)iron and tris-(naphthalen-2-yl iso-cyanide)(η4-tetra-phenyl-cyclo-penta-dienone)iron acetone hemisolvate [0.03%]
环戊二烯酮三异氰酸根铁复合物：三（2,6-二甲基苯异氰化物）（η⁴-四苯基环戊二烯酮）铁和三（萘-2-基异氰化物）（η⁴-四苯基环戊二烯酮）铁乙 ketone 半水合物的晶体结构及通用合成方法
André Bütikofer,Peter Chen
André Bütikofer
Irradiation of a toluene solution containing cyclo-penta-dienone tricarbonyl iron complexes and isocyanides with blue LEDs afforded the formation and isolation of 12 triisocyanide complexes, two of which, namely tris-(2,6-di-methyl-phenyl i...
Crystal structures and Hirshfeld surface analyses of (E)-1-[1-(4- tert-butyl-phen-yl)-2,2-di-chloro-ethen-yl]-2-phenyl-diazene, (E)-1-[1-(4- tert-butyl-phen-yl)-2,2-di-chloro-ethen-yl]-2-(4-methyl-phen-yl)diazene, (E)-1-[1-(4- tert-butyl-phen-yl)-2,2-di-chloro-ethen-yl]-2-(4-meth-oxy-phen-yl)diazene and (E)-1-[1-(4- tert-butyl-phen-yl)-2,2-di-chloro-eth [0.03%]
(E)-1-[1-(4-叔丁基苯基)-2,2-二氯乙烯基]-2-苯基偶氮苯、(E)-1-[1-(4-叔丁基苯基)-2,2-二氯乙烯基]-2-(4-甲基苯基)偶氮苯、(E)-1-[1-(4-叔丁基苯基)-2,2-二氯乙烯基]-2-(4-甲氧基苯基)偶氮苯的晶体结构和Hirshfeld面分析
Abel Maharramov,Namiq Q Shikhaliyev,Ayten Qajar et al.
Abel Maharramov et al.
The crystal structures and Hirshfeld surface analyses of four similar azo compounds are reported. (E)-1-[1-(4-tert-Butyl-phen-yl)-2,2-di-chloro-ethen-yl]-2-phenyl-diazene, C18H18Cl2N2, (I), and (E)-1-[1-(4-tert-butyl-phen-yl)-2,2-di-chloro-...
Crystal structure of 5-(β-d-gluco-pyran-osyl-thio)- N-(4-methyl-phen-yl)-1,3,4-thia-diazol-2-amine [0.03%]
5-(β-d-葡萄吡喃糖基硫)-N-(4-甲基苯基)-1,3,4-噻二唑-2-胺的晶体结构
Mamdouh A Abu-Zaied,Ali M S Hebishy,Galal H Elgemeie et al.
Mamdouh A Abu-Zaied et al.
In the structure of the title compound, C15H19N3O5S2, the bond lengths at the linking sulfur atom are significantly different [1.7473 (17) and 1.811 (2) Å], and the angle at the exocyclic nitro-gen atom is wide at 128.45 (18)°. The inter-...
Shaziyaparveen K Siddiqui,C V Ramana,Rajesh G Gonnade
Shaziyaparveen K Siddiqui
The title compound, 1-(4-bromo-phen-yl)but-3-yn-1-one, C10H7BrO, crystallizes in the monoclinic space group P21/n with one mol-ecule in the asymmetric unit. The structure displays a planar geometry. The crystal structure is consolidated by ...