Crystal structure and Hirshfeld surface analysis of (2 Z)-3-oxo- N-phenyl-2-[(1 H-pyrrol-2-yl)methylidene]butanamide monohydrate [0.03%]
(2Z)-3-氧代-N-苯基-2-[(1H-吡咯-2-基)亚甲基]丁酰胺单水合物的晶体结构和 Hirshfeld 表面分析
Ayten S Safarova,Ali N Khalilov,Mehmet Akkurt et al.
Ayten S Safarova et al.
In the title compound, C15H14N2O2·H2O, the 1H-pyrrole ring makes a dihedral angle of 59.95 (13)° with the phenyl ring. In the crystal, the mol-ecules are connected by C-H⋯O hydrogen bonds into layers parallel to the (020) plane, while tw...
Crystal structure reinvestigation and spectroscopic analysis of tricadmium orthophosphate [0.03%]
三镉正磷酸盐的晶体结构重新研究和光谱分析
Fatima-Zahra Cherif,Mhamed Taibi,Ali Boukhari et al.
Fatima-Zahra Cherif et al.
Single crystals of tricadmium orthophosphate, Cd3(PO4)2, have been synthesized successfully by the hydro-thermal route, while its powder form was obtained by a solid-solid process. The corresponding crystal structure was determined using X-...
Synthesis, characterization, crystal structure and Hirshfeld surface analysis of isobutyl 4-[4-(di-fluoro-meth-oxy)phen-yl]-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexa-hydro-quinoline-3-carboxyl-ate [0.03%]
异丁基 4-[4-(二氟甲氧基)苯基]-2,6,6-三甲基-5-氧代-1,4,5,6,7,8-六氢喹啉-3-羧酸酯的合成、表征、晶体结构及 Hirshfeld 表面分析
Sema Öztürk Yıldırım,Mehmet Akkurt,Gökalp Çetin et al.
Sema Öztürk Yıldırım et al.
In the title compound, C24H29F2NO4, which crystallizes in the ortho-rhom-bic Pca21 space group with Z = 4, the 1,4-di-hydro-pyridine ring adopts a distorted boat conformation, while the cyclo-hexene ring is in a distorted half-chair conform...
Crystal structure and Hirshfeld surface analysis of 10-hy-droxy-2-(4-meth-oxy-phen-yl)-3-oxo-2,3,3a,4,10,10a-hexa-hydro-1 H-9-thia-2-aza-cyclo-penta-[ b]fluorene-4-carb-oxy-lic acid dimethyl sulfoxide- d6 monosolvate [0.03%]
10-羟基-2-(4-甲氧基苯基)-3-氧代-2,3,3a,4,10,10a-六氢-1H-9-硫杂-2-氮杂环戊烷-[b]荧蒽-4-羧酸二甲亚砜-d6单溶剂化物的晶体结构和 Hirshfeld 表面分析
Gunay Z Mammadova,Elizaveta D Yakovleva,Pavel P Erokhin et al.
Gunay Z Mammadova et al.
In the title compound, C22H19NO5S·C2D6OS, the central six-membered ring has a slightly distorted boat conformation, while the fused pyrrolidine ring adopts an envelope conformation. These conformations are stabilized by O-H⋯O hydrogen bon...
Synthesis, structure and Hirshfeld surface analysis of 1,3-bis-[(1-octyl-1 H-1,2,3-triazol-4-yl)meth-yl]-1 H-benzo[ d]imidazol-2(3 H)-one [0.03%]
1,3-双-[(1-辛基-1H-1,2,3-三氮唑-4-基)甲基]-1H-苯并[d]咪唑-2(3H)-酮的合成，结构及 Hirshfeld 表面分析
Mustapha Zouhair,Lhoussaine El Ghayati,Hanae El Monfalouti et al.
Mustapha Zouhair et al.
The title mol-ecule, C29H44N8O, adopts a conformation resembling a two-bladed fan with the octyl chains largely in fully extended conformations. In the crystal, C-H⋯O hydrogen bonds form chains of mol-ecules extending along the b-axis dire...
Crystal structures of the isotypic complexes bis-(morpholine)-gold(I) chloride and bis-(morpholine)-gold(I) bromide [0.03%]
双(吗啉)金(Ⅰ)氯化物和双(吗啉)金(Ⅰ)溴化物的等构体 complexes 的晶体结构
Cindy Döring,Peter G Jones
Cindy Döring
The compounds bis-(morpholine-κN)gold(I) chloride, [Au(C4H9NO)2]Cl, 1, and bis-(morpholine-κN)gold(I) bromide, [Au(C4H9NO)2]Br, 2, crystallize isotypically in space group C2/c with Z = 4. The gold atoms, which are axially positioned at th...
Synthesis, crystal structure and properties of chlorido-tetra-kis-(pyridine-3-carbo-nitrile)-thio-cyanato-iron(II) [0.03%]
氯化四(吡啶-3-腈)硫氰酸铁(II)的合成、晶体结构及性质
Asmus Müller-Meinhard,Inke Jess,Christian Näther
Asmus Müller-Meinhard
Reaction of FeCl2·4H2O with KSCN and 3-cyano-pyridine (pyridine-3-carbo-nitrile) in ethanol accidentally leads to the formation of single crystals of Fe(NCS)(Cl)(3-cyano-pyridine)4 or [FeCl(NCS)(C6H4N2)4]. The asymmetric unit of this compo...
Synthesis and crystallographic characterization of 6-hydroxy-1,2-dihydropyridin-2-one [0.03%]
6-羟基-1,2-二氢吡啶-2-酮的合成及其晶体结构表征
Sara K Phillips,Savannah G Brancato,Samantha N MacMillan et al.
Sara K Phillips et al.
The title compound, C5H5NO2, is a hy-droxy-lated pyridine ring that has been studied for its involvement in microbial degradation of nicotinic acid. Here we describe its synthesis as a formic acid salt, rather than the standard hydro-chlori...
Crystal structure of polymeric bis-(3-amino-1 H-pyrazole)-cadmium dibromide [0.03%]
聚双(3-氨基-1H-吡唑)镉二溴化物的晶体结构
Iryna S Kuzevanova,Oleksandr S Vynohradov,Vadim A Pavlenko et al.
Iryna S Kuzevanova et al.
The reaction of cadmium bromide tetra-hydrate with 3-amino-pyrazole (3-apz) in ethano-lic solution leads to tautomerization of the ligand and the formation of crystals of the title compound, catena-poly[[di-bromido-cadmium(II)]-bis-(μ-3-am...
Crystal structure of S- n-octyl 3-(1-phenyl-ethyl-idene)di-thio-carbazate and of its bis-chelated nickel(II) complex [0.03%]
S-n-辛基-3-(1-苯基亚乙基)-二硫代卡巴腙及其双螯合ニ克尔(II)配合物的晶体结构研究
Sultana Shakila Khan,Md Belayet Hossain Howlader,Md Chanmiya Sheikh et al.
Sultana Shakila Khan et al.
The nitro-gen-sulfur Schiff base proligand S-n-octyl 3-(1-phenyl-ethyl-idene)di-thio-carbazate, C17H26N2S2 (HL), was prepared by reaction of S-octyl di-thio-carbamate with aceto-phenone. Treatment of HL with nickel acetate yielded the compl...