Crystal structure of μ3-tetra-thio-anti-monato-tris[(cyclam)zinc(II)] tetra-thio-anti-monate aceto-nitrile disolvate dihydrate showing Zn disorder over the cyclam ring planes (cyclam = 1,4,8,11-tetra-aza-cyclo-tetra-deca-ne) [0.03%]
μ3-四硫代抗坏血酸根三[(环己撑)-锌(II)]四硫代抗坏血酸根乙腈双溶剂化双水合物的晶体结构[Zn disorder在环平面上](cyclam = 1,4,8,11-四氮杂环十四碳)
Christian Näther,Felix Danker,Wolfgang Bensch
Christian Näther
Reaction of Zn(ClO4)2·6H2O with cyclam (cyclam = 1,4,8,11-tetra-aza-cyclo-tetra-decane, C10H24N4) and Na3SbS4 in an aceto-nitrile/water mixture led to the formation of crystals of the title compound, [Zn3(SbS4)(C10H24N4)3](SbS4)·2CH3CN·2...
A new pseudopolymorph of berberine chloride: crystal structure and Hirshfeld surface analysis [0.03%]
氯化小檗碱的新伪多形体：晶体结构和Hirshfeld表面分析
Tatiana Kornilova,Viktor Glebov,Raúl Castañeda et al.
Tatiana Kornilova et al.
A new pseudopolymorph of berberine, 9,10-dimeth-oxy-5,6-di-hydro-2H-7λ5-[1,3]dioxolo[4,5-g]iso-quinolino-[3,2-a]isoquinolin-7-ylium chloride methanol monosolvate, C20H18NO4 +·Cl-·CH3OH, was obtained during co-crystallization of berberine...
Synthesis and crystal structure of anti-10-butyl-10,11,22,23-tetra-hydro-9 H,21 H-5,8:15,12-bis(metheno)[1,5,11]tri-aza-cyclo-hexa-decino[1,16- a:5,6- a']di-indole [0.03%]
反式-10-丁基-9 H,21 H-5,8:15,12-双(甲撑)-[1,5,11]三氮杂环十二碳烯并[1,16-a:5,6-a']二吲哚的合成与晶体结构
Koji Kubono,Keita Tani,Yukiyasu Kashiwagi et al.
Koji Kubono et al.
The title compound, C33H33N3, is a carbazolophane, which is a cyclo-phane composed of two carbazole fragments. It has a planar chirality but crystallizes as a racemate in the space group P . The mol-ecule adopts an anti-configuration, in wh...
Crystal structure of di-μ-chlorido-bis-{chlorido-[(-)-5,6-pinenebi-pyridine]-cobalt(II)} aqua-dichlorido[(-)-5,6-pinenebi-pyridine]cobalt(II) [0.03%]
二氯化二(氯-顺式-5,6-蒎烯联吡啶合钴(II))水合二氯化顺式-5,6-蒎烯联吡啶合钴(II)的晶体结构
Massimo Varisco,Aurelien Crochet,Olimpia Mamula Steiner
Massimo Varisco
The crystal structure of [Co2Cl4(C17H18N2)2][CoCl2(C17H18N2)(H2O)] or [Co(L)Cl(μ-Cl)]2[Co(L)(Cl)2(OH2)], where L is the enanti-opure bidentate ligand (-)-5,6-pinenebi-pyridine (C17H18N2), has been determined. Crystals suitable for X-ray st...
Ninganayaka Mahesha,Haruvegowda Kiran Kumar,Hemmige S Yathirajan et al.
Ninganayaka Mahesha et al.
Six piperazinium salts, namely 4-(4-nitro-phenyl)-piperazin-1-ium 4-bromo-ben-zo-ate dihydrate, C10H14N3O2 +·C7H4BrO2 -·2H2O, (I), 4-(4-nitro-phenyl)-pi-per-a-zin-1-ium 4-iodo-benzoate dihydrate, C10H14N3O2 +·C7H4IO2 -·2H2O, (II), 4-(4-...
Syntheses, crystal structures and Hirshfeld surface analyses of bis-(2-mercaptobenzimidazole)-bromo- and iodo-copper(I) complexes [0.03%]
双(2-Mercaptobenzmidazole)溴化物和碘化物铜(I)配合物的合成、晶体结构和Hirshfeld面分析
Pipat Chooto,Saowanit Saithong,Weena Aemaeg et al.
Pipat Chooto et al.
The title complexes, bromidobis(2,3-dihydro-1H-1,3-benzodiazole-2-thi-one)copper(I), [CuBr(C7H6N2S)2] (1), and bis(2,3-dihydro-1H-1,3-benzodiazole-2-thione)iodidocopper(I) acetone monosolvate, [CuI(C7H6N2S)2]·CH3COCH3 (2), were prepared by...
4-[(Benzyl-amino)-carbon-yl]-1-methyl-pyridinium bromide hemihydrate: X-ray diffraction study and Hirshfeld surface analysis [0.03%]
4-[[（苄基氨基）羰基]-1-甲基吡啶溴化物半水合物的X射线衍射研究及Hirshfeld面分析
Vitalii V Rudiuk,Anna M Shaposhnik,Vyacheslav M Baumer et al.
Vitalii V Rudiuk et al.
The hemihydrate of 4-[(benzyl-amino)-carbon-yl]-1-methyl-pyridinium bromide, C14H15N2O+·Br-·0.5H2O, was studied by single-crystal and powder X-ray diffraction methods. In the asymmetric unit, two organic cations of similar conformation, t...
Crystal structure of bis-(ammonium) bis-[penta-aqua-(di-methyl-formamide)-zinc(II)] deca-vanadate tetra-hydrate [0.03%]
双（铵）四水双〔五水合锌(II)〕十钒酸盐的晶体结构
Arash Ebrahimi,Róbert Gyepes,Marek Bujdoš et al.
Arash Ebrahimi et al.
The crystalline product (NH4)2[Zn(C3H7NO)(H2O)5]2[V10O28]·4H2O was success-fully isolated from an H2O/DMF solvent combination by evaporation at ambient temperature. The salt crystallizes in the P21/n space group. Imidazole, initially used ...
Crystal structure and Hirshfeld surface analysis of 1-(tert-butyl-amino)-3-mesitylpropan-2-ol hemi-hydrate [0.03%]
1-(叔丁基氨基)-3-甲异丙苯基-2-丙醇半水合物的晶体结构和Hirshfeld面分析
Ali N Khalilov,Victor N Khrustalev,Tatiana A Tereshina et al.
Ali N Khalilov et al.
The title compound, 2C16H27NO·H2O, crystallizes in the monoclinic P21/c space group with two independent mol-ecules (A and B) in the asymmetric unit. In the crystal, mol-ecules A and B are linked through the water mol-ecules by inter-molec...
Crystal structures and electrochemical properties of nickel(II) complexes with N, N', N'', S-tetra-dentate Schiff base ligands [0.03%]
含N，N′，N″，S-四齿席夫碱配体的镍（II）配合物晶体结构和电化学性质研究
Masakazu Hirotsu,Junhei Sanou,Toyotaka Nakae et al.
Masakazu Hirotsu et al.
The thiol-ate nickel complexes {2-[({2-[(2-amino-ethyl-κN)(meth-yl)amino-κN]eth-yl}imino-κN)meth-yl]benzene-thiol-ato-κS}nickel(II) chloride, [Ni(C12H18N3S)]Cl (1), and [2-({[2-(piperazin-1-yl-κ2 N 1,N 4)eth-yl]imino-κN}meth-yl)benzen...