Synthesis and solid-state structures of a macrocyclic receptor based on the 2,6-bis(2-anilinoethynyl)pyridine scaffold [0.03%]
基于2,6-双(2-苯氨基乙炔基)吡啶的巨环受体的合成及其固态结构研究
Jeffrey M Engle,Pushpinder S Singh,Chris L Vonnegut et al.
Jeffrey M Engle et al.
A fluorescent macrocyclic anion receptor based on the 2,6-bis(2-anilinoethynyl)pyridine scaffold has been synthesized to investigate the mechanism of fluorescence quenching in this class of compounds. X-ray crystallography reveals that the ...
Stacks and clips: Uncanny similarities in the modes of self-assembly in tenary Ag(I) complexes with 1,2-diazines and chelating heteroarenes [0.03%]
三元银(i)配位物中含1,2-二氮杂茂和杂芳烃螯合体的自我装配模式的相似性:令人不安的相似之处
Yunus E Türkmen,Saikat Sen,Viresh H Rawal
Yunus E Türkmen
The first synthesis and structural elucidation of Ag(I) ternary complexes with 1,2-diazines and chelating heteroarenes have been described. Conserved modes of inter-cation Ag+⋯π and π⋯π stacking interactions result in near identical pa...
Effect of Ancillary Ligand on Electronic Structure as Probed by 51V Solid-State NMR Spectroscopy for Vanadium- o-Dioxolene Complexes [0.03%]
辅助配体对钒-o-二氧六环配合物电子结构的影响:通过51V固态NMR光谱探测
Olga Goncharova-Zapata,Pabitra B Chatterjee,Guangjin Hou et al.
Olga Goncharova-Zapata et al.
A series of vanadium(V) complexes with o-dioxolene (catecholato) ligands and an ancillary ligand, (N-(salicylideneaminato)ethylenediamine) (hensal), were investigated using 51V solid-state magic angle spinning NMR spectroscopy (51V MAS NMR)...
Crystallization of l-alanine in the presence of additives on a circular PMMA platform designed for metal-assisted and microwave-accelerated evaporative crystallization [0.03%]
圆型PMMA平台中金属辅助及微波加速蒸发法下助剂存在时L-丙氨酸结晶研究
Anginelle M Alabanza,Muzaffer Mohammed,Kadir Aslan
Anginelle M Alabanza
Crystallization of l-alanine in the presence of l-valine and l-tryptophan additives on a circular poly(methyl) methacrylate (PMMA) platform designed for Metal-Assisted and Microwave-Accelerated Evaporative Crystallization (MA-MAEC) techniqu...
Growth of oriented p-aminobenzoic acid crystals by directional freezing [0.03%]
定向冷冻法生长对位氨基苯甲酸单晶体的研究
Young Gun Ko,Peter X Ma
Young Gun Ko
Oriented long needle-like p-aminobenzoic acid (PABA) crystals are successfully prepared by directional freezing of PABA solution in this work. The width of the oriented crystals is controlled by changing the directional cooling rate, result...
Rediscovering Hydrogel-Based Double-Diffusion Systems for Studying Biomineralization [0.03%]
基于水凝胶的双扩散系统在生物矿化研究中的重新发现
Jason R Dorvee,Adele L Boskey,Lara A Estroff
Jason R Dorvee
For those seeking to model biomineralization in vitro, hydrogels can serve as excellent models of the extracellular matrix (ECM) microenvironment. A major challenge posed in implementing such systems is the logistics involved, from fundamen...
Rapid crystallization of L-arginine acetate on engineered surfaces using metal-assisted and microwave-accelerated evaporative crystallization() [0.03%]
金属助加速微波蒸发结晶技术在工程表面快速制备L-精氨酸乙酸盐晶体的研究()
Melissa A Pinard,Tsehai A J Grell,Danielle Pettis et al.
Melissa A Pinard et al.
We report the application of our newly described crystallization technique, which employs silver island films (SIFs) and microwave heating, to rapid crystallization of L-arginine acetate (LAA). Using our technique, LAA crystals (~ 1.2 mm in...
Md Alamgir Hossain,Musabbir A Saeed,Ganna Grynova et al.
Md Alamgir Hossain et al.
Structural analysis of sulfate complexes of two different azacryptands crystallized under identical conditions in the presence of methanol and water reveals that one methanol is selectively trapped in each cavity, assisted by the specific a...
Eue-Soon Jang,Jung-Hee Won,Young-Woon Kim et al.
Eue-Soon Jang et al.
Three different ZnO nanoplate arrays on Si-wafer were successfully synthesized at 95 °C from ZnO nanoparticles with modified surface by citrate anion. Shape, size, density, and orientation of the resulting nanoplates were dramatically chan...
Musabbir A Saeed,Jameskia J Thompson,Frank R Fronczek et al.
Musabbir A Saeed et al.