1-[(2-Bromo-phen-yl)di-phenyl-meth-yl]-3-(tri-fluorometh-yl)-1 H-pyrazole-1-(tri-phenyl-meth-yl)-3-(tri-fluoro-meth-yl)-1 H-pyrazole (0.638:0.362) [0.03%]
1-[(2-溴苯基)二苯甲基]-3-(三氟代甲基)-1H-吡唑与1-(三苯甲基)-3-(三氟代甲基)-1H-吡唑 (0.638:0.362)
Firudin I Guseinov,Aida I Samigullina,Tuncer Hökelek et al.
Firudin I Guseinov et al.
In the title compound, 0.638C23H16BrF3N2·0.362C23H17F3N2, the Br atom has been partially replaced by an H atom by reaction with NaH. In the crystal, pairwise C-H⋯Br hydrogen bonds link the mol-ecules into centrosymmetric dimers, enclosing...
Farkhod Raxmatovich Jumabaev,Avez Tuymuradovich Sharipov,Vazirakhon Khasanxoja Kizi Mannopova et al.
Farkhod Raxmatovich Jumabaev et al.
The manganese(II) coordination compound, [Mn(C8H13S2O2)2(H2O)2], with two bidentate α-lipoate ligands and two coordinating water mol-ecules, has been structurally characterized. The cantral MnII atom lies on a crystallographic twofold rota...
(3 Z)-4-Methyl-9-(4-methyl-benzene-sulfon-yl)- N-phenyl-3 H,9 H-thio-pyrano[3,4- b]indol-3-imine [0.03%]
(3Z)-4-甲基-9-(4-甲基苯磺酰)-N-苯基-3H,9H噻喃并吡咯并吲哚-3-亚胺
Benjamin Dassonneville,Heiner Detert,Dieter Schollmeyer
Benjamin Dassonneville
The title indolothiopyrane imine, C25H20N2O2S2, which was prepared by a [2 + 2 + 2] cycloaddition reaction, crystallizes with two molecules in the asymmetric unit. Both adopt the shape of a staircase with two steps, consolidated by intramol...
tert-Butyl [(4-fluoro-3-isopropoxyisoxazol-5-yl)meth-yl](phenyl-sulfon-yl)carbamate [0.03%]
4-氟-3-异丙氧基异唑-5-甲基苯磺酰氨基碳酸叔丁酯
Mohd Abdul Fatah Abdul Manan,David B Cordes
Mohd Abdul Fatah Abdul Manan
The title compound, C18H23FN2O6S, a new derivative of a fluoro-isoxazole containing sulfonamide functionality has been structurally characterized. The C-S-N-Cipr and C-S-N-Ccarb (ipr = 3-isopropoxyisoxazole, carb = carbamate) torsion angles...
4,12-Diselena-5,6,13,14-tetra-aza-tri-cyclo-[9.3.0.03,7]tetra-deca-1(11),3(7),5,13-tetra-ene [0.03%]
4,12-二硒代-5,6,13,14-四氮杂三环[9.3.0.0~(3,7)]十四-1(11),3(7),5,13- tetraene
Dieter Schollmeyer,Heiner Detert
Dieter Schollmeyer
In the title com-pound, C8H8N4Se2, two almost planar 1,2,3-selena-diazo-les are annulated to a cyclo-octa-1,4-diene with a boat-chair conformation, giving the mol-ecule a butterfly shape. ...
2'-Amino-5'-benzoyl-5-bromo-6'-methyl-2-oxo-spiro-[indoline-3,4'-pyran]-3'-carbo-nitrile [0.03%]
2'-氨基-5'-苯甲酰基-5-溴-6'-甲基-2-氧代螺(吲哚啉-3,4'-吡喃)-3'-腈
Farid N Naghiyev,Tuncer Hökelek,Victor N Khrustalev et al.
Farid N Naghiyev et al.
In the title compound, C21H14BrN3O3, the indoline ring system is almost planar, while the pyran ring is in flattened-boat conformation. In the crystal, N-H⋯O and N-H⋯N hydrogen bonds link the mol-ecules, enclosing R 2 2(8) and R 2 2(12) r...
Bis[5-(anthracen-9-ylmeth-yl)-1,5,9-tri-aza-cyclododecan-1-ium] tetra-chlorido-zincate [0.03%]
5-[9-（蒽甲基）]-1,5,9-三氮杂环十二碳-1-𬭩双离子四氯化锌盐
Yoshimi Ichimaru,Koichi Kato,Wanchun Jin et al.
Yoshimi Ichimaru et al.
A crystalline salt comprising two monoprotonated polyamine ligands and one tetra-chloro-zincate(II) anion was prepared, (C24H32N3)2[ZnCl4], and its crystal structure was analyzed and compared with those of structurally related compounds bea...
Heiner Detert,Dieter Schollmeyer
Heiner Detert
The crystal structure of cyclo-decynone oxime, C10H15NO, is reported. Two twist-boat-shaped cyclo-alkynes are centrosymmetrically connected via oxime hydrogen bridges. Deformation of the alkyne unit results from ring strain. ...
2-Amino-6-nitro-1,3-benzo-thia-zol-3-ium 3-carb-oxy-4-hy-droxy-benzene-1-sulfonate [0.03%]
2-氨基-6-硝基-1,3-苯并噻唑鎓 3-甲氧基-4-羟基苯磺酸盐
Joseph Tsemeugne,Didier Forest Kouganou Djossu,Dieter Schollmeyer et al.
Joseph Tsemeugne et al.
In the title salt, C7H6N3O2S+·C7H5O6S-, the cation is protonated at the thia-zole N atom and the dihedral angle between the nitro group and its attached benzene ring is 3.6 (4)°. In the anion, the sulfonate group is deprotonated and the d...
2-Amino-4-ferrocenyl-5-oxo-5,6,7,8-tetra-hydro-4 H-chromene-3-carbo-nitrile monohydrate [0.03%]
2-氨基-4- ferrocen基-5-氧代-5，6，7，8-四氢-4H-色烯-3-甲腈单水合物
Carren Nyapola,David O Juma,Sizwe J Zamisa et al.
Carren Nyapola et al.
In the title hydrate, [Fe(C5H5)(C15H13N2O2)]·H2O, the pendent ferrocenyl substituent is significantly rotated against the chromene backbone, with a torsion angle of 56.8 (2)°. Rotational disorder is observed in one of the Cp rings of the ...