Jean Guillaume Ducreux,James A Kaduk,Anja Dosen et al.
Jean Guillaume Ducreux et al.
The crystal structure of 5-amino-levulinic acid hydro-chloride (systematic name: 4-carb-oxy-2-oxobutan-1-aminium chloride), C5H10NO3 +·Cl-, has been solved and refined using synchrotron X-ray powder diffraction data, and optimized using de...
Bis(μ-1,4-di-hydro-pyridin-4-one-κ2 O: O)di-μ-perchlorato-κ4 O: O'-bis-[aqua-(1,4-di-hydro-pyridin-4-one-κ O)copper(II)] tetra-aqua-bis-(1,4-di-hydropyridin-4-one-κ O)copper(II) tetra-kis-(perchlorate) 1,4-di-hydro-pyridin-4-one disolvate [0.03%]
二氧杂环戊并吡啶鎓四氯化铜(II)二水合物
Mark M Turnbull,Christopher P Landee,Jan L Wikaira
Mark M Turnbull
The reaction of copper(II) perchlorate hexa-hydrate with 4-pyridone and pyrazine in 1-propanol serendipitously yielded crystals of the solvated title double salt, [Cu(C5H5NO)2(H2O)4][Cu2(ClO4)2(C5H5NO)4(H2O)2](ClO4)4·2C5H5NO, as a biproduc...
7- tert-Butyl-1,3-bis-(eth-oxy-meth-yl)pyrene [0.03%]
7-叔丁基-1,3-双(乙氧亚甲基)菲rine"structural_correction"
Tetsuji Moriguchi,Misa Sasaki,Noriko Miyoshi
Tetsuji Moriguchi
In the mol-ecular structure of the title compound, C26H30O2, the two eth-oxy-methyl side arms are twisted from the almost planar pyrene system by 29.85 (17) and 15.16 (18)°. In the crystal, adjacent mol-ecules are arranged in pairs that ma...
2-Meth-oxy-4-[1-(4-meth-oxy-phen-yl)-4,5-diphenyl-1 H-imidazol-2-yl]phenol [0.03%]
2-甲氧基-4-[1-(4-甲氧基苯基)-4,5-二苯基-1H-咪唑-2-基]苯酚
Seeralan Nagaraj,Nagarajan Loganathan
Seeralan Nagaraj
The title compound, C29H24N2O3, was synthesized via a four-component Debus-Radziszewski reaction, involving benzil, amine, aldehyde and ammonium acetate. The OH group of the vanillin substituent forms both an intra-molecular and an inter-mo...
Di-chlorido-bis-(3-{[(pyridin-2-yl)methyl-idene]amino}-benzoic acid-κ2 N, N')cobalt(II) methanol monosolvate monohydrate [0.03%]
二氯化二(3-({[吡啶-2-基]亚甲基}氨基)苯甲酸-κ2NN')合钴(II)甲醇一溶剂化水合物
Olga Yu Vassilyeva,Vladimir N Kokozay,Brian W Skelton
Olga Yu Vassilyeva
The ortho-rhom-bic (space group Pna21) unit cell of the title compound, [CoCl2(C13H10N2O2)2]·CH3OH·H2O, contains eight complex mol-ecules, four A and four B, along with sixteen solvent mol-ecules of crystallization. The two independent Co...
trans-Di-aqua-bis-(pyridin-2-yl thio-phen-2-yl ketone-κ2 N, O)nickel(II) bis-(tetra-fluorido-borate) [0.03%]
二吡啶-2-基硫苯-2-酮-N,O-双酮合镍(II)二水合物双四氟硼酸盐
Barry L Westcott,Gary S Nichol
Barry L Westcott
The complex title salt, [Ni(C10H7NOS)2(H2O)2](BF4)2, has monoclinic symmetry (space group P21/c) with the central NiII atom located at an inversion center. The coordination environment around the NiII atom is pseudo-octa-hedral with bonding...
(E)-1-(3,3'-Dimeth-oxy-4'-{[(E)-4-nitro-benzyl-idene]amino}-[1,1'-biphen-yl]-4-yl)- N-(4-nitro-phen-yl)methanimine [0.03%]
(N)-(4-硝基苯基)-N'-[3,3'-二甲氧基-4'-((E)-4-硝基苯甲亚氨基)茋-4-基]亚甲胺][(E)-1-(3,3'-二methoxy-4'-(4-硝基苯甲亚氨基)[1,1'-联苯]-4-基]-N-(4-硝基苯基)甲醛亚胺
Ouafa Boukhemis,Ahlem Linda Boulkedid,Mehdi Boutebdja et al.
Ouafa Boukhemis et al.
The title compound, C28H22N4O6, crystallizes with one half-mol-ecule in the asymmetric unit centered on a twofold rotation axis located at the midpoint of the central C-C bond. The structure is non-planar overall, with nearly planar anisole...
A polymorph of N'-[(4-hy-droxy-phen-yl)methyl-idene]pyridine-4-carbohydrazide [0.03%]
N'-[(4-羟基苯基)甲酰基]异烟酸肼的一种多晶型物
Lincy Tom,Jerry P Jasinski,Victoria A Smolenski et al.
Lincy Tom et al.
The synthesis and single-crystal X-ray diffraction analysis of a polymorphic form of the isoniazid derivative N'-[(4-hy-droxy-phen-yl)methyl-idene]pyridine-4-carbohydrazide, C13H11N3O2, are reported, revealing that both the mol-ecular confo...
{5,15-Bis[3,5-bis-(6'-methyl-2,2'-bipyridyl-6-yl)phen-yl]-10,20-di-phenyl-porphyrin}zinc(II) 1,2-di-meth-oxy-ethane 0.296-solvate [0.03%]
5,15-双[3,5-双(6'-甲基-2,2'-二吡啶-6-基)苯基]-10,20-二苯基锌(ii)卟啉乙二醇单甲醚溶剂化物
Aguri Akitomi,Yuta Kato,Yosuke Hosoya et al.
Aguri Akitomi et al.
In the title compound, [Zn(C88H60N12)]·0.296C4H10O2, the porphyrin macrocycle is essentially planar, with the Zn atom located in the plane on an inversion centre. The non-substituted and bi-pyridine-bearing phenyl rings are twisted with re...
On the crystal structure of tri-benzyl-tin(IV) iodide, Bz3SnI: a correction [0.03%]
关于三苯基锡(IV)碘化物的晶体结构的更正:Bz3SnI
Nadia-Ammane Reuter,Hans Reuter
Nadia-Ammane Reuter
Tri-benzyl-iodido-tin(IV), [Sn(C7H7)3I], has been prepared and its crystal structure determined in order to clarify some discrepancies in a previous report. The compound does not crystallize in the rhombohedral space group R3 as originally ...