10-(4-Fluoro-phen-yl)-4-[(4-fluoro-phen-yl)amino]-5-phenyl-5,8,9,10-tetra-hydro-pyrimido[4,5- b]quin-olin-6(7 H)-one [0.03%]
1-(4-氟苯基)-4-[(4-氟苯基)氨基]-10-甲基-5-苯基-5,8,9,10-四氢吡啶并[4,5-b]喹啉-6(7H)-酮
Sizwe J Zamisa,Adesola A Adeleke,Bernard Omondi
Sizwe J Zamisa
The asymmetric unit of the title compound, C29H22F2N4O, consists of one mol-ecule in which the pyrimidinyl and anilinyl units exhibit near coplanarity, subtending a dihedral angle of 10.22 (7)°. In contrast, the di-hydro-pyridine and pheny...
Rao M Uppu,Frank R Fronczek
Rao M Uppu
In the title compound, C8H8ClNO2, the acetamide substituent is twisted out of the phenyl plane, forming a dihedral angle of 58.61 (7)°. In the extended structure, each mol-ecule donates two hydrogen bonds [N-H⋯O(carbon-yl) and O-H⋯O(carb...
Phuong-Truc T Pham,Mamoun M Bader
Phuong-Truc T Pham
[This corrects the article DOI: 10.1107/S2414314624012434.]. Keywords: addendum; crystal structure; curcumin...
Published Erratum
IUCrData. 2025 Aug 28;10(Pt 8):x250635. DOI:10.1107/S2414314625006352 2025
Di-μ-hydroxido-bis-[iodido-diphenyl-tin(IV)]-1,3-di-methyl-imidazolidin-2-one (1/2) [0.03%]
1,3-二甲基咪唑烷-2-酮合四（苯锡）二μ-羟基双（碘）合物
Hans Reuter
Hans Reuter
The title compound, di-μ-hydroxido-bis-[iodido-diphenyl-tin(IV)]-1,3-di-methyl-imidazolidin-2-one (1/2), [Sn(C6H5)2I(OH)]·2C6H12N2O, represents only the second example in the dimeric diorganotin(IV)-hydroxide-halide solvates [R 2Sn(OH)Hal...
tert-Butyl 5-{2-[2-(N-ethynyl-4-methyl-benzene-sulfonamido)-phen-yl]ethyn-yl}furan-2-carboxyl-ate [0.03%]
叔丁基5-{2-[2-(N-乙炔基-4-甲基苯磺酰胺)-苯基]乙炔基}呋喃-2-甲酸酯
Benjamin Dassonneville,Heiner Detert,Dieter Schollmeyer
Benjamin Dassonneville
The crystal structure of an o,N-dialkynyl-tosyl-aniline, C26H23NO5S, is presented. Two essentially planar and nearly parallel branches are connected to the aniline unit and the angle between the alkynes amounts to 26 (4)°. Weak intra-molec...
5-Methyl-2-nitro-aniline [0.03%]
5-甲基-2-硝基苯胺
Lily Samson,Lydia Banwart,Sajan Silwal et al.
Lily Samson et al.
The bond lengths and angles within the title mol-ecule, C7H8N2O2, conform to average values for other 5-substituted-2-nitro-anilines, and with those calculated by a DFT geometry optimization. The short C-NH2 bond length of 1.3469 (12) Å is...
Rochdi Ghallab,Amina Kemmouche,Mehdi Boutebdja et al.
Rochdi Ghallab et al.
The title compound, (C6H14NO2)2[SnCl6]·2H2O, features l-leucinium cations adopting extended conformations, which maximizes the separation between the methyl groups [-CH(CH3)2] and the polar NH3 + and COOH moieties. Additionally, an intra-m...
Firudin I Guseinov,Tuncer Hökelek,Elena V Shuvalova et al.
Firudin I Guseinov et al.
The asymmetric unit of the title compound, C3H4N4O2, contains two coplanar mol-ecules (A and B) completely located on mirror planes. In the crystal, N-H⋯O, N-H⋯N, C-H⋯O and C-H⋯N hydrogen bonds link the mol-ecules into sheets parallel t...
catena-Poly[[[aqua-copper(II)]-μ-hydroxido-κ2 O: O-μ-[3-(4 H-1,2,4-triazol-4-yl)benzoato]-κ2 N 1: N 2] monohydrate] [0.03%]
聚[[四羟基-μ3-1,2,4-三氮唑-3,5-二苯甲酸-μ-氢氧化氧阴离子-二(氢氧化)铜(II)]一水合物]
Xiao-Yu Li,Ye Zhou,Hong-Can Wang et al.
Xiao-Yu Li et al.
In the title compound, {[Cu(C9H6N3O2)(OH)(H2O)]·H2O]} n , the Cu2+ cation is situated on a twofold rotation axis and is coordinated by two triazole N atoms from two different 3-(4H-1,2,4-triazol-4-yl)benzoate (3-tba) ligands, by two hydrox...
(Nitrito-κ O)(nitro-κ N)(nitrosyl-κ N)bis-(tri-phenylphosphane-κ P)rhodium(III) [0.03%]
硝基三(三苯磷烷-κP)（硝酰基-κN）（亚硝基-κO）合铑(III)
Daniel R Albert,Michael Gau,Edward Rajaseelan
Daniel R Albert
The structure of the title compound, [Rh(NO)(NO2)2(C18H15P)2] or [Rh(NO)(NO2)(ONO)(PPh3)2], has been determined by single-crystal X-ray diffraction. A previous report of the title compound showed it crystallized in a monoclinic space group ...