Crystal structure of an indium-salicyl-hydroximate complex cation: [In4(H2shi)8(H2O)6](NO3)4·8.57H2O [0.03%]
铟-水杨醛羟亚胺配合物阳离子晶体结构:[In4(H2shi)8(H2O)6](NO3)4·8.57H2O
Ozha A Aziz,Matthias Zeller,Curtis M Zaleski
Ozha A Aziz
The synthesis and crystal structure for the title compound, hexa-aqua-hexa-kis(μ-2-hy-droxy-benzene-carbo-hydrox-a-mato)bis-(2-hy-droxy-benzene-carbo-hydrox-a-m-ato)tetra-indium(III) tetra-nitrate 8.57-hydrate + unknown solvent, [In4(H2shi...
Syntheses and crystal structures of 4-(4-meth-oxy-phen-yl)piperazin-1-ium 4-methyl-benzoate monohydrate and bis-[4-(4-meth-oxy-phen-yl)piperazin-1-ium] benzene-1,2-di-carboxyl-ate [0.03%]
4-(4-甲氧基苯基)哌啶-1-ium 4-甲基苯甲酸单水合物和双[4-(4-甲氧基苯基)哌啶-1-ium] 苯-1,2-二羧酸盐的合成和晶体结构
Holehundi J Shankara Prasad,Devaraju,Vinaya et al.
Holehundi J Shankara Prasad et al.
Co-crystallization of N-(4-meth-oxy-phen-yl)piperazine with 4-methyl-benzoic acid and with benzene-1,2-di-carb-oxy-lic acid yields the salts 4-(4-meth-oxy-phen-yl)piperazin-1-ium 4-methyl-benzoate monohydrate, C11H17N2O+·C8H7O2 -·H2O (I),...
Synthesis, X-ray diffraction study, analysis of inter-molecular inter-actions and mol-ecular docking of ethyl 1-(3-tosyl-quinolin-4-yl)piperidine-4-carboxyl-ate [0.03%]
合成、X射线衍射研究、分子间相互作用及乙基1-(3-托磺酸基喹啉-4-基)哌啶-4-甲酸酯的分子对接分析
Yevhenii Vaksler,Halyna V Hryhoriv,Sergiy M Kovalenko et al.
Yevhenii Vaksler et al.
The title compound, C24H26N2O4S, can be obtained via two synthetic routes. According to our investigations, the most suitable way is by the reaction of ethyl 2-bromo-acetate with sodium tosyl-sulfinate in dry DMF. It was crystallized from m...
Classroom experiments with artificial sweeteners: growing single crystals and simple calorimetry [0.03%]
代糖的课堂实验：单晶生长和简单热容测量
Johan Wouters,Luc Van Meervelt
Johan Wouters
An easily accessible experimental set-up to grow large single crystals of two sweeteners readily available in supermarkets, erythritol and xylitol, is described. The crystallization of these compounds illustrates the principles of crystalli...
Effect of methyl-ene versus ethyl-ene linkers on structural properties of tert-butyl and mesityl bis-(imidazolium) bromide salts [0.03%]
甲基和乙基连接体对叔丁基和三苯甲基双咪唑
Emily S Thompson,Elisa M Olivas,Adrian Torres et al.
Emily S Thompson et al.
The crystal structures of ligand precursor bis-(imidazolium) salts 1,1'-methyl-enebis(3-tert-butyl-imidazolium) dibromide monohydrate, C15H26N4 +·2Br-·H2O or [ tBuNHC2Me][Br]2·H2O, 1,1'-(ethane-1,2-di-yl)bis-(3-tert-butyl-imidazolium) di...
Crystal structure and Hirshfeld surface analysis of ethyl 2'-amino-5-bromo-3'-cyano-6'-methyl-2-oxo-spiro-[indoline-3,4'-pyran]-5'-carboxyl-ate [0.03%]
乙基2'-氨基-5-溴-3'-氰基-6'-甲基-2-氧代螺-[, ]-[吲哚并[3,4-]吡喃]-5'-羧酸酯的晶体结构及Hirshfeld面分析
Farid N Naghiyev,Victor N Khrustalev,Nikolai U Venskovsky et al.
Farid N Naghiyev et al.
The crystal used for structure determination contained, along with the title compound, C17H14BrN3O4, an admixture [0.0324 (11)] of its 7-bromo isomer. The 2,3-di-hydro-1H-indole ring system is nearly planar, while the conformation of the 4H...
Crystal structure of N-butyl-2,3-bis-(di-cyclo-hexyl-amino)-cyclo-propeniminium chloride benzene monosolvate [0.03%]
N-丁基-2,3-双(二环己基氨基)环丙烯亚铵氯化物苯溶剂化物的晶体结构
Gaby M Muñoz Sánchez,Michael J Zdilla
Gaby M Muñoz Sánchez
N-Butyl-2,3-bis-(di-cyclo-hexyl-amino)-cyclo-propenimine (1) crystallizes from benzene and hexa-nes in the presence of HCl as a mono-benzene solvate of the hydro-chloride salt, [1H]Cl·C6H6 or C31H54N3 +·Cl-·C6H6, in the P21/n space group...
Crystal structure and Hirshfeld surface analysis of 4-(3-meth-oxy-phen-yl)-2,6-di-phenyl-pyridine [0.03%]
4-(3-甲氧基苯基)-2,6-二苯基吡啶的晶体结构和Hirshfeld面分析
Dong Cheng,Xiang-Zhen Meng,Fuyu Tian et al.
Dong Cheng et al.
The title compound, C24H19NO, was obtained via the reaction of (1E,2E)-3-(3-meth-oxy-phen-yl)-1-phenyl-prop-2-en-1-one with ethyl 2-oxo-propano-ate, using NH4I as a catalyst. The compound crystallizes in the monoclinic space group I2/a. In ...
Crystal structures of the Lewis acid-base adducts {[(C6H11)2N]3Ti- LB}+[MeB(C6F5)3]-·1.5C7H8; LB = (C6H5)3PO (1), p-F-C6H4CN (2) [0.03%]
路易斯酸碱加合物{[(C6H11)2N]3Ti-LB}+[MeB(C6F5)3]-·1.5C7H8的晶体结构;LB = (C6H5)3PO(1), p-F-C6H4CN(2)
Kerstin Fitschen,Nils Frerichs,Zainab Yusufzadeh et al.
Kerstin Fitschen et al.
The reaction of [(C6H11)2N]3Ti-CH3 with the Lewis acid B(C6F5)3, followed by addition of the Lewis bases (C6H5)3PO and p-F-C6H4CN led to the complex salts tris-(di-cyclo-hexyl-amido)(tri-phenyl-phosphine oxide)titanium methyl-tris(penta-flu...
Incorporation of in situ generated 3,3'-(sulfane-diyl)bis-(1-methyl-1,3-imidazolidine-2-thione) into a one-dimensional CuI coordination polymer with sulfur-bridged {CuI 4S10} n central cores [0.03%]
通过原位生成的3,3'-(硫代二亚乙基)双(1-甲基-1,3-咪唑烷-2-硫酮)构筑具有{CuIS10}n心核的一维CuI配位聚合物
Tarlok Singh Lobana,Ray J Butcher,Jerry P Jasinski
Tarlok Singh Lobana
The reaction of [Cu(CH3CN)4](BF4) with 1-methyl-1,3-imidazolidine-2-thione {SC3H4(NMe)NH}, under aerobic conditions at room temperature, yielded an unusual one-dimensional coordination polymer, namely, catena-poly[[[(1-meth-yl-1,3-imidazoli...