Syntheses and crystal structures of benzyl N'-[(E)-2-hydroxybenzylidene]hydrazinecarboxylate and benzyl N'-[(E)-5-bromo-2-hydroxybenzylidene]hydrazinecarboxylate [0.03%]
苯甲酰肼缩氨基硫脲和5-溴苯甲酰肼缩氨基硫脲的合成及晶体结构测定
Vinaya,Yeriyur B Basavaraju,Beliyaiah Lakshmana et al.
Vinaya et al.
Benzyl N'-[(E)-2-hydroxybenzylidene]hydrazinecarboxylate, C15H14N2O3 (I) and benzyl N'-[(E)-5-bromo-2-hydroxybenzylidene]hydrazinecarboxylate (II), C15H13BrN2O3, have been synthesized by the reaction of either 2-hy-droxy-benzaldehyde or 5-b...
Hélène Cattey,Gilles Boni,Sylvie Pourchet et al.
Hélène Cattey et al.
The title compound, C13H16O3 [GE-isoEu; systematic name: 2-({2-meth-oxy-4-[(E)-1-propen-1-yl]phen-oxy}meth-yl)oxirane], which crystallizes in the triclinic P space group, was synthesized in one step from iso-eugenol, a bio-based phenyl-prop...
Synthesis and crystal structure of 3-phenyl-1,4,2-di-thia-zole-5-thione [0.03%]
3-苯基-1,4,2-二噻唑-5-硫酮的合成与晶体结构测定
Melbourne J Schriver,Tanner George,Jason D Masuda
Melbourne J Schriver
In the title compound, C8H5NS3, the dihedral angle between the heterocyclic ring and the phenyl ring is 2.62 (5)°. In the extended structure, aromatic π-π stacking between the 1,4,2-di-thia-zole-5-thione moiety and the phenyl ring is obs...
Synthesis and crystal structures of 1-benzoyl-4-(4-nitro-phen-yl)piperazine and 1-(4-bromo-benzo-yl)-4-phenyl-piperazine at 90 K [0.03%]
1-苯甲酰基-4-(对硝基苯基)哌嗪和1-(4-溴苯甲酰基)-4-苯基哌嗪的合成及晶体结构研究
Sreeramapura D Archana,Haruvegowda Kiran Kumar,Holehundi J Shankara Prasad et al.
Sreeramapura D Archana et al.
Synthesis and crystal structures of 1-benzoyl-4-(4-nitro-phen-yl)piperazine, C17H17N3O3, (I) and 1-(4-bromo-benzo-yl)-4-phenyl-piperazine, C17H17BrN2O, (II) are described. Compounds I and II crystallize in the ortho-rhom-bic and monoclinic ...
Synthesis and structure of clozapine N-oxide hemi(hydro-chloride): an infinite hydrogen-bonded poly[ n]catenane [0.03%]
氯化克洛扎平-N-氧化物半水合物的合成与结构：一个无限氢键缔合的多维链分子结构
Phillip L van der Peet,Rohan D Joyce,Holger Ott et al.
Phillip L van der Peet et al.
The structure of the title compound, 2C18H19ClN4O·HCl or (CNO)2·HCl (C36H39Cl3N8O2), at 100 K has tetra-gonal (I4/m) symmetry. The dihedral angle between the benzene rings of the fused ring system of the CNO mol-ecule is 40.08 (6)° and t...
Crystal structure and Hirshfeld surface analysis of 3-({4-[(4-cyano-phen-oxy)carbon-yl]phen-oxy}carbon-yl)phenyl 4-(benz-yloxy)-3-chloro-benzoate [0.03%]
3-({4-[(4-氰基苯氧基)羰基]苯氧基}羰基)苯基 4-(苯氧基)-3-氯苯甲酸酯的晶体结构和Hirshfeld面分析
S Selvanandan,H Anil Kumar,H T Srinivasa et al.
S Selvanandan et al.
The title compound, C35H22ClNO7, is a non-liquid crystal with a bent-shaped mol-ecule. The dihedral angles between adjacent aromatic rings in the mol-ecule (starting from the cyano-benzene ring) are 72.61 (2), 87.69 (4), 64.08 (2) and 88.23...
Crystal structure of catena-poly[[[bis-(1-benzyl-imidazole-κ N)copper(II)]-μ-sulfato-κ2 O: O'-[tetra-kis-(1-benzyl-imidazole-κ N)copper(II)]-μ-sulfato-κ2 O: O'] N, N-di-methyl-formamide disolvate dihydrate] [0.03%]
一苯甲基咪唑为配体的铜(I)和铜(II)硫酸盐配合物的晶体结构(N，N-二甲基甲酰胺溶剂化物单水合物)
Nareekarn Meebua,Wanatchaporn Pentes,Kittipong Chainok et al.
Nareekarn Meebua et al.
The title one-dimensional copper(II) coordination polymer, {[Cu(SO4)(C10H10N2)3]·C3H7NO·H2O} n or {[Cu(bzi)3(μ-O2SO2)]·H2O·DMF} n (bzi = 1-benz-yl-imidazole, C10H10N2; DMF = N,N-di-methyl-formamide, C3H7NO), is constructed by monodenta...
Crystal structure of bis-{4-[(4-methyl-benz-yl)-oxy]- N'-(4-methyl-benzyl-idene)benzohydrazidato}nickel(II) [0.03%]
六水合硝酸二氨基合镍(II)·2-硫脲复合物的晶体结构
Md Hasan Al Banna,Md Belayet Hossain Howlader,Ryuta Miyatake et al.
Md Hasan Al Banna et al.
In the title complex, [Ni(C23H21N2O2)2], the central NiII atom is located on an inversion centre and exhibits a slightly distorted square-planar N2O2 coordination environment. A trans-configuration of the N,O chelating ligands results from ...
Crystal structure, PIXEL calculations of inter-molecular inter-action energies and solid-state characterization of the herbicide isoxaflutole [0.03%]
异噁草氟晶体结构、分子间相互作用能量的PIXEL计算和固态表征
Jascha Schinke,Thomas Gelbrich,Ulrich J Griesser
Jascha Schinke
In the isoxaflutole mol-ecule {systematic name: (5-cyclo-propyl-1,2-oxazol-4-yl)[2-(methyl-sulfon-yl)-4-(tri-fluoro-meth-yl)phen-yl]methanone; C15H12F3NO4S}, the 1,2-oxazole and methanone fragments form an almost coplanar unit, whereas the ...
Inter-molecular hydrogen bonding in N-methyl- N'-(pyridin-2-yl)benzene-1,2-di-amine [0.03%]
N-甲基-N'-吡啶并[2,3-b]苯-1,2-二胺的分子间氢键作用
Gavin Collis,Alex Bilyk,Ueno Kazanori et al.
Gavin Collis et al.
The structure of N-methyl-N'-(pyridin-2-yl)benzene-1,2-di-amine, C12H13N3, at 123 K has ortho-rhom-bic (Pna21) symmetry. The title compound displays an unexpected proton-splitting pattern when studied by 1H NMR spectroscopy. The X-ray cryst...