The structures of eleven (4-phen-yl)piperazinium salts containing organic anions [0.03%]
含有有机酸根的十一例(4-苯基)哌啶
Sreeramapura D Archana,Haruvegowda Kiran Kumar,Hemmige S Yathirajan et al.
Sreeramapura D Archana et al.
Eleven (4-phen-yl)piperazinium salts containing organic anions have been prepared and structurally characterized, namely, 4-phenyl-piperazin-1-ium 4-fluoro-benzoate monohydrate, C10H15N2 +·C7H4FO2 -·H2O, 1; 4-phenyl-piperazin-1-ium 4-brom...
Structures of dicobalt and dinickel 4,4'-bi-phenyldi-carboxyl-ate di-hydroxide, M 2(O2CC6H4C6H4CO2)(OH)2, M = Co and Ni, and di-ammonium 4,4'-bi-phenyldi-carboxyl-ate from powder diffraction data [0.03%]
来自粉晶数据的二价钴和镍以及硫酸氢二(4-羧基苯偶氮)
Joshua D Vegetabile,James A Kaduk
Joshua D Vegetabile
The triclinic structures of poly[(μ4-4,4'-bi-phenyldi-carboxyl-ato)di-μ-hydroxido-dicobalt], [Co2(C14H8O4)(OH)2] n , and poly[(μ4-4,4'-bi-phenyldi-carboxyl-ato)di-μ-hydroxido-dinickel], [Ni2(C14H8O4)(OH)2] n , were established using lab...
Synthesis, crystal structure and Hirshfeld surface analysis of (1 H-benzimidazol-2-yl)(morpholin-4-yl)methane-thione [0.03%]
(1H-苯并咪唑-2-基)(吗啉-4-基)甲烷硫化物的合成、晶体结构及Hirshfeld面分析
Lukmonjon Z Mutalliev,Sirojiddin Abdullaev,Nasiba Pirnazarova et al.
Lukmonjon Z Mutalliev et al.
The title compound, C12H13N3OS, was synthesized via the Willgerodt-Kindler method. The benzimidozole moiety is essentially planar (r.m.s. deviation = 0.0084 Å). The thio-amide group is inclined by 54.80 (14)° to the benzimidazole ring sys...
Crystal structure of ethyl 4-[(4-methyl-benz-yl)-oxy]benzoate [0.03%]
乙基4-[[（4-甲基苯基）甲氧基]氧代]苯甲酸酯的晶体结构
Md Hasan Al Banna,Md Rezaul Haque Ansary,Ryuta Miyatake et al.
Md Hasan Al Banna et al.
The title compound, C17H18O3, crystallizes with three mol-ecules in the asymmetric unit. The mol-ecules differ in the conformation related to the eth-oxy group and in the orientation of the two phenyl rings, one of which has the eth-oxy gro...
Synthesis, crystal structure and Hirshfeld surface analysis of tert-butyl N-acetyl-carbamate [0.03%]
叔丁基N-乙酰氨基甲酸酯的合成、晶体结构及Hirshfeld面分析
Aly Dawa El Mestehdi,Moctar Abba,Mohamed Lemine El Housseine et al.
Aly Dawa El Mestehdi et al.
This article reports a practical synthesis of tert-butyl acetyl-carbamate, C7H13NO3, from N-Boc-thio-acetamide and the study of its crystal structure. The reaction proceeds in the presence of natural phosphate as a catalyst, with excellent ...
The methanol and ethanol solvates of 4-glutarato- N, N-diiso-propyl-tryptamine [0.03%]
LSD的谷氨酸二异丙胺盐的甲醇和乙醇溶剂合物
Marilyn Naeem,Barbara E Bauer,Andrew R Chadeayne et al.
Marilyn Naeem et al.
The solid-state structures of two solvated forms of 4-glutarato-N,N-diiso-propyl-tryptamine were determined by single-crystal X-ray diffraction, namely, 5-[(3-{2-[bis(propan-2-yl)azaniumyl]ethyl}-1H-indol-4-yl)oxy]-5-oxopentanoate meth-anol...
Crystal structure of 2,5-di-hydroxy-terephthalic acid from powder diffraction data [0.03%]
基于粉末衍射数据的2,5-二羟基对苯二甲酸晶体结构
Joshua D Vegetabile,James A Kaduk
Joshua D Vegetabile
The crystal structure of anhydrous 2,5-dhy-droxy-terephthalic acid, C8H6O6, was solved and refined using laboratory X-ray powder diffraction data, and optimized using density functional techniques. The published structure of 2,5-di-hydroxy-...
Qi-Ming Qiu,Li Yan,Jian-Biao Song
Qi-Ming Qiu
The solvothermal reaction of H3BO3, sodium tert-butoxide, Rb2CO3 and pyridine led to a new alkaline metal borate hexa-rubidium hexa-hydroxy-dodeca-borate dihydrate, Rb6[B12O18(OH)6]·2H2O. Its structure contains a large cyclic dodeca-oxobor...
Syntheses and crystal structures of the ethanol, acetonitrile and diethyl ether Werner clathrates bis-(iso-thio-cyanato-κ N)tetra-kis-(3-methyl-pyridine-κ N)nickel(II) [0.03%]
乙醇、乙腈和二乙醚合抱剂双(异硫氰酸根)-四(3-甲基吡啶-N)镍(II)的合成与晶体结构测定
Christoph Krebs,Inke Jess,Christian Näther
Christoph Krebs
The reaction of nickel(II)thio-cyanate with 3-methyl-pyridine (3-picoline; C6H7N) in different solvents leads to the formation of crystals of bis-(iso-thio-cyanato-κN)tetra-kis-(3-methyl-pyridine-κN)nickel(II) as the ethanol disolvate, [N...
Crystal structure of MgK0.5[B6O10](OH)0.5·0.5H2O, poly[dimagnesium potassium bis(hexa-borate) hy-droxide monohydrate] [0.03%]
镁钾双(六硼酸酯)氢氧化物单水合物的晶体结构 MgK0.5[B6O10](OH)0.5·0.5H2O poly[dimagnesi-um potassium bis(hexaborate)] hydride monohydrate
Qi-Ming Qiu,Jian-Biao Song
Qi-Ming Qiu
The solvothermal reaction of H3BO3, KCF3SO3, Mg(CF3SO3)2 and pyridine led to a new alkali- and alkaline-earth-metal borate, MgK0.5[B6O10](OH)0.5·0.5H2O. Its structure features an intricate three-dimensional framework built from [B6O13]8- c...