Synthesis, crystal structure and Hirshfeld surface analysis of bis-[4-(2-amino-eth-yl)morpholine-κ2 N, N']di-aqua-nickel(II) dichloride [0.03%]
二水合四乙二胺合镍(II)二氯化物的合成、晶体结构和Hirshfeld面分析
Balasubramanian Chidambaranathan,Settu Sivaraj,Pandy Vijayamathubalan et al.
Balasubramanian Chidambaranathan et al.
The title coordination compound, [Ni(C6H14N2O)2(H2O)2]Cl2, was synthesized by mixing 4-(2-amino-eth-yl)morpholine and nickel chloride in double-distilled water. The asymmetric unit comprises one half of an NiII cation (located on an inversi...
Hemant P Yennawar,Anna Sigmon,Eleanora Margulis
Hemant P Yennawar
The crystal structures of racemic mixtures of three new flavanone-hydrazones in the centrosymmetric space group (P ), are reported. The structures of (±,E)-N'-[5,7-dihy-droxy-2-(4-hy-droxy-phen-yl)chroman-4-yl-idene]-2-(naphthalen-1-yl)ace...
Leonard Rössner,Yurii Prots,Yuri Grin et al.
Leonard Rössner et al.
Quaternary (Sn,Pb,Bi)Pt was synthesized by melting of the elements in an evacuated silica glass ampoule. The crystal structure was established by single-crystal X-ray diffraction and adopts an atomic arrangement of the NiAs type with additi...
Structures of S-(pyridin-2-yl) 4-nitro-benzo-thio-ate, S-(pyridin-2-yl) 4-methyl-benzo-thio-ate and S-(pyridin-2-yl) 4-meth-oxy-benzo-thio-ate: building blocks for low-symmetry multifunctional tetra-pyrroles [0.03%]
S-(吡啶-2-基)-4-硝基苯并噻化合物、S-(吡啶-2-基)-4-甲基苯并噻化合物和S-(吡啶-2-基)-4-甲氧基苯并噻化合物的结构：合成低对称多功能四吡咯单元的构建模块
Harry C Sample,Brendan Twamley,Mathias O Senge
Harry C Sample
The crystal structures of three S-(pyridin-2-yl) benzo-thio-esters with varying para-phenyl substituents are presented, namely, S-(pyridin-2-yl) 4-nitro-benzo-thio-ate (1, C12H8N2O3S), S-(pyridin-2-yl) 4-methyl-benzo-thio-ate (2, C13H11NO2S...
Crystal structures of di-μ-chlorido-bis-({(E)-5-(ethyl-amino)-4-methyl-2-[(pyridin-2-yl)diazen-yl]phen-o-lato}copper(II)) and chlorido-bis-(1,10-phen-anthroline)copper(II) chloride tetra-hydrate [0.03%]
二氯化二{(E)-5-(乙基氨基)-4-甲基-2-[吡啶-2-基偶氮]苯酚合}铜(II)和氯化双(1,10-菲啰啉)铜(II)单氯化物四水合物的晶体结构
Alex Meier,Mohammad Rasel Mian,Siyu Ou et al.
Alex Meier et al.
The dark-red title complex crystallized from an equimolar methanol solution of (E)-5-(ethyl-amino)-4-methyl-2-[(pyridin-2-yl)diazen-yl]phenol and CuCl2(phen) (phen = 1,10-phenanthroline) as a centrosymmetric dimer, [CuCl(C14H15N4O)]2. The C...
Synthesis, crystal structure and thermal properties of di-μ-iodido-bis-[bis-(2-chloro-pyrazine-κ N)copper(I)] [0.03%]
二碘化双(2-氯吡嗪)铜(I)的合成、晶体结构及其热学性能研究
Christian Näther,Inke Jess
Christian Näther
Reaction of copper(I) iodide in pure 2-chloro-pyrazine leads to the formation of a few crystals of the title compound, [Cu2I2(C4H3ClN2)4] or (CuI)2(2-chloro-pyrazine)4, which was characterized by single-crystal X-ray diffraction. In its cry...
Crystal structure and Hirshfeld surface analysis of isopropyl 4-[2-fluoro-5-(tri-fluoro-meth-yl)phen-yl]-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexa-hydro-quinoline-3-carboxyl-ate [0.03%]
异丙基4-[2-氟-5-(三氟甲基)苯基]-2,6,6-三甲基-5-氧代-1,4,5,6,7,8-六氢喹啉-3-羧酸酯的晶体结构和Hirshfeld面分析
Sema Öztürk Yıldırım,Mehmet Akkurt,Gökalp Çetin et al.
Sema Öztürk Yıldırım et al.
In the title compound, C23H25F4NO3, the 1,4-di-hydro-pyridine ring adopts a distorted boat conformation, while the cyclo-hexene ring is almost showing a half-chair conformation. In the crystal, inter-molecular N-H⋯O hydrogen bonds connect ...
Crystal structure of a methyl benzoate quadruple-bonded dimolybdenum complex [0.03%]
甲基苯甲酸四价二钼配合物的晶体结构
Lillian Dawson Bass,Jessie H Lee,McKenzie C Lilygren et al.
Lillian Dawson Bass et al.
Quadruple-bond dimolybdenum complexes provide invaluable insight into the two-electron bond, with structural chemistry providing a foundation for examination of bond properties. The synthesis and solid-state structure of the quadruple-bonde...
Bart Kahr
Bart Kahr
There are about 100 chemical elements, and 200 space groups, rounding to the nearest hundreds. The elements, by virtue of the iconic periodic table, which hangs in schoolrooms worldwide, are part of our common culture. Few on the outside of...
Synthesis, crystal structure and properties of bis-(iso-seleno-cyanato-κ N)tetra-kis-(4-meth-oxy-pyridine-κ N)cobalt(II) [0.03%]
二氯化四(4-甲氧基吡啶-N)双(iso-硒氰酸根-N)合钴的合成、晶体结构和性质研究
Christian Näther,Inke Jess
Christian Näther
Reaction of CoCl2·6H2O with KNCSe and 4-meth-oxy-pyridine in water led to the formation of the title compound, [Co(NCSe)2(C6H7NO)4] or Co(NCSe)2(4-meth-oxy-pyridine)2, which was characterized by single-crystal X-ray diffraction. Its asymme...