Synthesis and structure of 4-hy-droxy- N-iso-propyl-tryptamine (4-HO-NiPT) and its precursors [0.03%]
4-羟基-N-异丙基多巴胺(4-HO-NiPT)的合成及其前体的结构
Uroš Laban,Marilyn Naeem,Andrew R Chadeayne et al.
Uroš Laban et al.
The title compound, 4-hy-droxy-N-iso-propyl-tryptamine (4) or 4-HO-NiPT (systematic name: 3-{2-[(propan-2-yl)amino]-eth-yl}-1H-indol-4-ol), C13H18N2O, was synthesized in three steps from 4-benzyl-oxyindole (1) (systematic name: 4-phen-oxy-1...
Enanti-opure (S)-butan-2-yl N-(4- x-phen-yl)thio-carbamates, x = NO2, OCH3, F, and Cl [0.03%]
(R)-或(S)-2-丁基-N-[4-(x代苯基)]硫代甲酰胺，x=NO₂,OCH₃,F和Cl
Werner Kaminsky,Max Kaganyuk
Werner Kaminsky
The structures of (S)-butan-2-yl N-(4-nitro-phen-yl)thio-carbamate, C11H14N2O3S, (I), (S)-butan-2-yl N-(4-meth-oxy-phen-yl)thio-carbamate, C12H17NO2S, (II), (S)-butan-2-yl N-(4-fluoro-phen-yl)thio-carbamate, C11H14FNOS, (III), and (S)-butan...
Crystal structures of three homologues with increasing ring size: 2-meth-oxy-4-(thio-phen-2-yl)-5,6,7,8-tetra-hydro-quinoline-3-carbo-nitrile, 2-meth-oxy-4-(thio-phen-2-yl)-6,7,8,9-tetra-hydro-5 H-cyclo-hepta-[ b]pyridine-3-carbo-nitrile and 2-meth-oxy-4-(thio-phen-2-yl)-5,6,7,8,9,10-hexa-hydrocyclo-octa[ b]pyridine-3-carbo-nitrile [0.03%]
三种增加环大小的同系物的晶体结构：2-甲氧基-4-(硫苯-2-基)-5,6,7,8-四氢喹啉-3-腈，2-甲氧基-4-(硫苯-2-基)-6,7,8,9-四氢-5H-环庚并吡啶-3-腈和2-甲氧基-4-(硫苯-2-基)-5,6,7,8,9,10-六氢化环辛并吡啶-3-腈
Ali M S Hebishy,Galal H Elgemeie,Lobna M Gouda et al.
Ali M S Hebishy et al.
The title compounds, C15H14N2OS (1a), C16H16N2OS (1b), and C17H18N2OS (1c), form a homologous series in which the size of the saturated ring increases from six- to eight-membered (with four, five and six methyl-ene groups respectively). For...
Synthesis, crystal structure and Hirshfeld surface analysis of the hybrid salt bis-(2-methyl-imidazo[1,5- a]pyridin-2-ium) tetra-chlorido-manganate(II) [0.03%]
双(2-甲基咪唑并[1,5-a]吡啶-2-鎓)四氯化锰(II)的合成、晶体结构和Hirshfeld面分析
Olga Yu Vassilyeva,Elena A Buvaylo,Vladimir N Kokozay et al.
Olga Yu Vassilyeva et al.
The 0-D hybrid salt bis-(2-methyl-imidazo[1,5-a]pyridin-2-ium) tetra-chlorido-manganate(II), (C8H9N2)2[MnCl4] or [L]2[MnCl4], consists of discrete L + cations and tetra-chlorido-manganate(II) anions. The fused heterocyclic rings in the two ...
Crystal structure, Hirshfeld surface analysis and DFT study of (5 E,5' E,6 Z,6' Z)-6,6'-[ethane-1,2-diyl-bis(aza-nylyl-idene)]bis-{5-[2-(4-fluoro-phen-yl)hydra-zono]-3,3-di-methyl-cyclo-hexa-none} 2.5-hydrate [0.03%]
(5E,5'E,6Z,6'Z)-6,6'-[乙烷-1,2-二基双(氮杂亚氨基)]双-{5-[2-(4-氟苯基)肼基]-3,3-二甲基环己酮}半水合物的晶体结构、Hirshfeld面分析和DFT研究
Malahat Musrat Kurbanova,Md Serajul Haque Faizi,Emine Berrin Cinar et al.
Malahat Musrat Kurbanova et al.
The title compound, C30H34F2N6O2·2.5H2O, was obtained by condensation of 2-[2-(4-fluoro-phen-yl)hydrazono]-5,5-di-methyl-cyclo-hexan-1,3-dione with ethyl-enedi-amine in ethanol and crystallized as a 1:2.5 hydrate in space group C2/c. The t...
Crystal structure of trimeth-yl({tris-[(phenyl-sulfan-yl)meth-yl]sil-yl}meth-oxy)silane and Hirshfeld surface analysis of 3-bromo-2,2-bis-(bromo-meth-yl)propan-1-ol [0.03%]
三甲基({tris[（苯硫基）甲基]硅基}甲氧基)硅烷的晶体结构和3-溴-2,2-双(溴甲基)丙-1-醇的Hirshfeld表分析
Jan Frederick Wappelhorst,Jonathan Wattenberg,Carsten Strohmann
Jan Frederick Wappelhorst
Trimeth-yl({tris-[(phenyl-sulfan-yl)meth-yl]sil-yl}meth-oxy)silane (3), C26H32OS3Si, is a new ligand for transition-metal coordination chemistry derived from 3-bromo-2,2-bis-(bromo-meth-yl)propan-1-ol (1), C5H9Br3O, through silylation and f...
Syntheses, crystal structures and thermal properties of catena-poly[cadmium(II)-di-μ-bromido-μ-pyridazine-κ2 N 1: N 2] and catena-poly[cadmium(II)-di-μ-iodido-μ-pyridazine-κ2 N 1: N 2] [0.03%]
[镉(Ⅱ)－双桥联溴－双桥联吡啶酮]多聚链的合成、晶体结构和热学性能研究[CdBr2(C5H4N2)]n与[Cdi(C5H4N2)]n
Christian Näther,Inke Jess
Christian Näther
The reactions of cadmium bromide and cadmium iodide with pyridazine (C4H4N2) in ethanol under solvothermal conditions led to the formation of crystals of [CdBr2(pyridazine)] n (1) and [CdI2(pyridazine)] n (2), which were characterized by si...
Felix Eder,Matthias Weil
Felix Eder
Na3Te2(FeO4)3 or Na3Te2Fe3O12, tris-odium ditellurium(VI) triiron(III) dodeca-oxide, was obtained in the form of single-crystals under hydro-thermal conditions. Na3Te2(FeO4)3 adopts the garnet structure type in space group Ia d and comprise...
Crystal structures of (12 E)-12-(4-benzyl-idene)-7,7,16-trimethyl-3-(4-methyl-phen-yl)-1-oxa-16-aza-tetra-cyclo-[11.2.1.02,11.04,9]hexa-deca-2(11),4(9)-dien-5-one and (12 E)-12-(4-bromo-benzyl-idene)-73-(4-bromo-phen-yl)-,7,16-trimethyl-10-oxa-16-aza-tetra-cyclo-[11.2.1.02,11.04,9]hexa-deca-2(11),4(9)-dien-5-one [0.03%]
(12E)-12-(4-苯甲亚烯基)-7,7,16-三甲基-3-(4-甲基苯基)-1-氧代-16-氮杂十七环[11.2.1.02,11.04,9]十五-2(11),4(9)二烯-5-酮和(12E)-12-(4-溴苯甲亚烯基)-73-(4-溴苯基)-7,16-三甲基-10-氧代-16-氮杂十七环[11.2.1.02,11.04,9]十五-2(11),4(9)二烯-5-酮的晶体结构
C Selva Meenatchi,R Vishnupriya,J Suresh et al.
C Selva Meenatchi et al.
The title compounds, C32H35NO2, (I), and C30H29Br2NO2, (II), differ by the presence of a bromine atom instead of a methyl atom in the para position of two benzene rings of compound (II). The two compounds have a structural overlap r.m.s. de...
rac-1-(4- tert-Butyl-phen-yl)-5-ethyl-4-ferrocenyl-5-hy-droxy-1 H-pyrrol-2(5 H)-one [0.03%]
1-(4-特丁基苯基)-5-乙基-4-铁ocene-5-羟基-1H-吡咯-2(5H)-酮
Tobias Biletzki,Helmar Görls,Wolfgang Imhof
Tobias Biletzki
The title compound, [Fe(C5H5)(C21H24NO2)], which is produced by the oxidation of 1-(4-tert-butyl-phen-yl)-2-ethyl-3-ferrocenyl-pyrrole, crystallizes as a racemic mixture in the centrosymmetric space group P21/n. The central heterocyclic pyr...