Synthesis and crystal structure of a new copper(II) complex based on 5-ethyl-3-(pyridin-2-yl)-1,2,4-triazole [0.03%]
基于5-乙基-3-(吡啶-2-基)-1,2,4-三唑的铜(ii)配合物的合成及晶体结构
Yuliia P Petrenko,Dmytro M Khomenko,Roman O Doroshchuk et al.
Yuliia P Petrenko et al.
The title compound, bis-[μ-3-ethyl-5-(pyridin-2-yl)-1H-1,2,4-triazol-1-ido]bis[acetato-(di-methyl-formamide)-copper(II)], [Cu2(C9H9N4)2(C2H3O2)2(C3H7NO)2] or [Cu2(L Et)2(OAc)2(dmf)2], is a triazolate complex, which contains two 3-(2-pyrid-...
Mohan M Bhadbhade,Jiabin Gao,Anne M Rich et al.
Mohan M Bhadbhade et al.
Duloxetine hydro-chloride (trade name Cymbalta) is marketed as a single enanti-omer (S)-N-methyl-3-(naphthalen-1-yl-oxy)-3-(thio-phen-2-yl)propyl-am-in-ium chloride, C18H20NOS+·Cl-, which is twice as effective as the (R)-enanti-omer in ser...
Synthesis and crystal structure of catena-poly[[[aqua-{2-[(E)-(1-cyano-2-imino-2-meth-oxy-ethyl-idene)hydrazin-yl]benzene-sulfonato}-sodium]-di-μ-aqua] dihydrate] [0.03%]
一水合四水合双亚氨基-2-(1-氰基-2-甲氧亚甲基亚胺基乙叉基)-重氮苯磺酸钠的合成和晶体结构分析
Vusala A Aliyeva,Fargana S Aliyeva,Mehmet Akkurt et al.
Vusala A Aliyeva et al.
In the polymeric title compound, {[Na(C10H9N4O4S)(H2O)3]·2H2O} n , sixfold coordinated Na+ cations are linked into a chain parallel to [010] by sharing common water mol-ecules. Next to the four bridging water mol-ecules, each Na+ cation of...
Crystal structure of bis-[4-(all-yloxy)- N'-(but-2-en-1-yl-idene)benzohydrazidato]nickel(II) [0.03%]
镍(II)双[4-(全氢氧基)-N'-(丁-2-烯-1-亚基)苯胲酸盐]晶体结构
Sultana Shakila Khan,Md Belayet Hossain Howlader,Md Chanmiya Sheikh et al.
Sultana Shakila Khan et al.
In the title complex, [Ni(C14H15N2O2)2], the nickel(II) atom exhibits a square-planar coordination geometry, being coordinated by two negatively charged N,O chelating ligands in a trans configuration, with the metal located on a crystallogr...
Crystal structure of 3-(benzo[ d]thia-zol-2-yl)-6-methyl-2 H-chromen-2-one [0.03%]
3-(苯并[d]噻唑-2-基)-6-甲基-2H-色烯-2-酮的晶体结构
Amira E M Abdallah,Galal H Elgemeie,Peter G Jones
Amira E M Abdallah
The mol-ecule of the title compound, C17H11NO2S, is almost planar, with an inter-planar angle of 3.01 (3)° between the benzo-thia-zole and chromene ring systems. A short intra-molecular S⋯O=C contact of 2.727 (2) Å is observed. The cryst...
Crystal structure and Hirshfeld surface analysis of 1,6-di-amino-2-oxo-4-(thio-phen-2-yl)-1,2-di-hydro-pyridine-3,5-dicarbo-nitrile [0.03%]
1,6-二氨基-2-氧代-4-(硫苯-2-基)-1,2-二氢吡啶并〔3，5〕二腈的晶体结构和Hirshfeld面分析
Farid N Naghiyev,Victor N Khrustalev,Mehmet Akkurt et al.
Farid N Naghiyev et al.
The asymmetric unit of the title compound, C11H7N5OS, contains two independent mol-ecules (1 and 2). The thio-phene ring in mol-ecule 2 is rotationally disordered (flip disorder) by ca 180° (around the single C-C bond, to which it is attac...
Crystal structure and Hirshfeld surface analysis of bis-(μ-4- tert-but-oxy-4-oxobut-2-en-2-olato)bis-[(4- tert-but-oxy-4-oxobut-2-en-2-olato)ethano-lzinc(II)] [0.03%]
四叔丁氧基巴豆酸根桥联锌化合物的晶体结构及Hirshfeld面分析
Olherd O Shtokvysh,Viktoriya V Dyakonenko,Lyudmila I Koval et al.
Olherd O Shtokvysh et al.
The mol-ecular and crystal structure of the title binuclear Zn2+ complex, [Zn2(C8H13O3)4(C2H5OH)2], with enolated anionic tert-butyl-aceto-acetate and ethanol was analysed. The coordination polyhedra of the Zn atoms are distorted octa-hedra...
Crystal structure and Hirshfeld surface analysis of 2,2'-[(3,5-di- tert-butyl-4-hy-droxy-phen-yl)methanedi-yl]bis-(3-hy-droxy-5,5-di-methyl-cyclo-hex-2-en-1-one) [0.03%]
2,2'-[(3,5-二-特丁基-4-羟基苯基)甲烷二基]双(3-羟基-5,5-二甲基环己-2-烯-1-酮)的晶体结构和Hirshfeld面分析
Ali N Khalilov,Victor N Khrustalev,Larissa V Aleksandrova et al.
Ali N Khalilov et al.
In the title compound, C31H44O5, mol-ecules are connected by O-H⋯O and C-H⋯O hydrogen bonds, forming hydrogen-bonded zigzag chains running along the b axis and parallel to the (001) plane. The mol-ecular packing is stabilized by van der W...
Crystal structure of N-[3-(benzo[ d]thia-zol-2-yl)-6-bromo-2 H-chromen-2-yl-idene]-4-methyl-benzenamine [0.03%]
N-[3-(苯并[d]噻唑-2-基)-6-溴-2H-色烯-2-基亚甲基]-4-甲基苯胺的晶体结构
Amira E M Abdallah,Galal H Elgemeie,Peter G Jones
Amira E M Abdallah
The title compound, C23H15BrN2OS, was the unexpected product in an attempted synthesis of the isomeric 3-(benzo[d]thia-zol-2-yl)-6-bromo-1-p-tolyl-quinolin-2(1H)-one. The Cchromene=N-C angle is wide [125.28 (8)°]. The benzo-thia-zole and c...
Crystal structure and Hirshfeld analysis of trans-di-iodido-bis-[(methyl-sulfan-yl)benzene-κ S]platinum(II) [0.03%]
茋配位的二碘化铂(II)晶体结构及其Hirshfeld面分析
Annika Schmidt,Isabelle Jourdain,Michael Knorr et al.
Annika Schmidt et al.
The title complex, [PtI2(C7H8I2)2], represents a further example of a square-planar PtII-di-thio-ether complex. It crystallizes in the monoclinic space group P21/c. Additional Hirshfeld analyses indicate a C-H⋯π inter-action along the [01...