Crystal structures of two formamidinium hexa-fluorido-phosphate salts, one with batch-dependent disorder [0.03%]
两种六氟磷酸式胺盐的晶体结构，其中一个具有批次依赖无序特性
Michelle C Neary,Peter W R Corfield,Sean R Parkin et al.
Michelle C Neary et al.
Syntheses of the acyclic amidinium salts, morpholino-formamidinium hexa-fluorido-phosphate [OC4H8N-CH=NH2]PF6 or C5H11N2O+·PF6 -, 1, and pyrrolidinoformamidinium hexa-fluorido-phosphate [C4H8N-CH= NH2]PF6 or C5H11N2 +·PF6 -, 2, were carri...
New copper carboxyl-ate pyrene dimers: synthesis, crystal structure, Hirshfeld surface analysis and electrochemical characterization [0.03%]
新的铜羧酸吡啶二聚体：合成、晶体结构、Hirshfeld表面分析及电化学特征化的研究
Vianca C Nogué-Guzmán,Alejandro Burgos-Suazo,Javier O Rivera-Reyes et al.
Vianca C Nogué-Guzmán et al.
Two new copper dimers, namely, bis-(dimethyl sulfoxide)-tetra-kis-(μ-pyrene-1-carboxyl-ato)dicopper(Cu-Cu), [Cu2(C17H9O2)4(C2H6OS)2] or [Cu2(pyr-COO-)4(DMSO)2] (1), and bis-(di-methyl-formamide)-tetra-kis-(μ-pyrene-1-carboxyl-ato)dicopper...
Crystal structure and Hirshfeld surface analysis of dieth-yl (3a S,3 a 1 R,4 S,5 S,6 R,6a S,7 R,9a S)-3a1,5,6,6a-tetra-hydro-1 H,3 H,4 H,7 H-3a,6:7,9a-di-epoxy-benzo[ de]isochromene-4,5-di-carboxyl-ate [0.03%]
(DE)-3a,6:7,9a-二环氧苯并[de]异色烯-4,5-二酸的晶体结构和Hirshfeld表面分析
Nurlana D Sadikhova,Zeliha Atioğlu,Narmina A Guliyeva et al.
Nurlana D Sadikhova et al.
In the title compound, C18H22O7, two hexane rings and an oxane ring are fused together. The two hexane rings tend toward a distorted boat conformation, while the tetra-hydro-furan and di-hydro-furan rings adopt envelope conformations. The o...
Crystal structure and Hirshfeld surface analysis of 3-benzyl-2-[bis(1 H-pyrrol-2-yl)methyl]thiophene [0.03%]
3-苄基-2-[双(1H-吡咯-2-基)甲基]噻吩的晶体结构和 Hirshfeld 表面分析
Nurlana D Sadikhova,Zeliha Atioğlu,Narmina A Guliyeva et al.
Nurlana D Sadikhova et al.
In the title compound, C20H18N2S, the asymmetric unit comprises two similar mol-ecules (A and B). In mol-ecule A, the central thio-phene ring makes dihedral angles of 89.96 (12) and 57.39 (13)° with the 1H-pyrrole rings, which are bent at ...
Crystal structure of 2-[(5-amino-1-tosyl-1 H-pyrazol-3-yl)-oxy]-1-(4-meth-oxy-phen-yl)ethan-1-one 1,4-dioxane monosolvate [0.03%]
2-[(5-氨基-1-对甲苯磺酰基-1H-吡唑-3-基)氧代]-1-(4-甲氧基苯基)乙酮1,4-二氧六环单溶剂合物的晶体结构
Nadia H Metwally,Galal H Elgemeie,Peter G Jones
Nadia H Metwally
In the structure of the title compound, C19H19N3O5S·C4H8O2, the two independent dioxane mol-ecules each display inversion symmetry. The pyrazole ring is approximately parallel to the aromatic ring of the oxy-ethanone group and approximatel...
Temperature-dependent solid-state phase transition with twinning in the crystal structure of 4-meth-oxy-anilinium chloride [0.03%]
晶体结构中4-甲氧基苯胺氯化物的温度依赖性固态相变及类晶转变
Rao M Uppu,Sainath Babu,Frank R Fronczek
Rao M Uppu
At room temperature, the title salt, C7H10NO+·Cl-, is ortho-rhom-bic, space group Pbca with Z' = 1, as previously reported [Zhao (2009 ▸). Acta Cryst. E65, o2378]. Between 250 and 200 K, there is a solid-state phase transition to a twinne...
Crystal structure and Hirshfeld surface analysis of 2-picolyllithium·3thf [0.03%]
2-吡啶基锂·3thf的晶体结构和希施菲尔德表面分析
Tristan Mairath,Annika Schmidt,Carsten Strohmann
Tristan Mairath
In the title compound, (2-methyl-idene-1,2-di-hydro-pyridinium-κN)tris-(tetra-hydro-furan-κO)lithium, [Li(C6H6N)(C4H8O)3], the lithium ion adopts a distorted LiNO3 tetra-hedral coordination geometry and the 2-picolyl anion adopts its enam...
Synthesis and crystal structures of two solvates of 1-{[2,6-bis-(hy-droxy-meth-yl)-4-methyl-phen-oxy]meth-yl}-3,5-bis-{[(4,6-di-methyl-pyridin-2-yl)amino]meth-yl}-2,4,6-tri-ethyl-benzene [0.03%]
1-{[2,6-双（羟甲基）-4-甲基苯氧基}甲基]-3,5-双-{[(4,6-二甲基吡啶-2-基)氨基]甲基}-2,4,6-三乙基苯的两种溶剂化物的合成和晶体结构
Manuel Stapf,Ute Schmidt,Wilhelm Seichter et al.
Manuel Stapf et al.
In the crystal structures of the formamide monosolvate (1a) and the n-propanol/H2O solvate/hydrate (1b) of the title compound, C38H50N4O3 (1), the tripodal host mol-ecule adopts a conformation in which the substituents attached to the centr...
Synthesis, crystal structure and Hirshfeld surface analysis of di-aqua-bis-(o-phenyl-enedi-amine-κ2N, N')nickel(II) naphthalene-1,5-di-sulfonate [0.03%]
二水合-o-苯烯二胺-镍(II)萘-1,5-二磺酸
Jabbor R Suyunov,Khayit Kh Turaev,Bekmurod Kh Alimnazarov et al.
Jabbor R Suyunov et al.
The reaction of o-phenyl-enedi-amine (OPD), sodium naphthalene1,5-di-sulfonate (Na2NDS) and nickel sulfate in an ethanol-water mixture yielded the title compound, [Ni(OPD)2(H2O)2]·NDS or [Ni(C6H8N2)2(H2O)2](C10H6O6S2). This salt consists o...
Synthesis and crystal structure of 2-(anthracen-9-yl)-1-(tert-butyl-dimethyl-sil-yl)-3,6-di-hydro-1λ4,2λ4-aza-borinine [0.03%]
2-(蒽-9-基)-1-(叔丁基二甲基硅烷基)-3,6-二氢-1λ4,2λ4-氮杂aborinine的合成与晶体结构
Philipp J Gliese,Yannik Appiarius,Tarek Scheele et al.
Philipp J Gliese et al.
The title compound, C24H30BNSi (I), is an asymmetric 1,2,3,6-tetra-hydro-1,2-aza-borinine consisting of a BN-substituted cyclo-hexa-diene analog with a B-anthracenyl substituent. A ring-closing metathesis with subsequent substitution of the...