Synthesis and crystal structures of boryl ortho-silylaryl tri-fluoro-methane-sulfonates [0.03%]
硼基邻硅芳基三氟甲烷磺酸酯的合成及其晶体结构研究
Fredrik Barnå,Matic Hribersek,Andreas Orthaber et al.
Fredrik Barnå et al.
We report the synthesis and structural characterization of three crystalline borylated ortho-silylaryl tri-fluoro-methane-sulfonates: 5-(4,4,5,5-tetra-methyl-1,3,2-dioxaborolan-2-yl)-2-(tri-methyl-sil-yl)phenyl tri-fluoro-methane-sulfonate,...
An unexpected tautomer: synthesis and crystal structure of N-[6-amino-4-(methyl-sulfan-yl)-1,2-di-hydro-1,3,5-triazin-2-yl-idene]benzenesulfonamide [0.03%]
一个意外的互变异构体：N-[6-氨基-4-(甲基硫代)-1,2-二氢-1,3,5-三嗪-2-亚基]苯磺酰胺的合成及晶体结构分析
Reham A Mohamed-Ezzat,Galal H Elgemeie,Peter G Jones
Reham A Mohamed-Ezzat
The title compound, C10H11N5O2S2, consists of an unexpected tautomer with a protonated nitro-gen atom in the triazine ring and a formal exocyclic double bond C=N to the sulfonamide moiety. The ring angles at the unsubstituted nitro-gen atom...
JUAMI, the joint undertaking for an African materials institute: building materials science research collaborations and capabilities between continents [0.03%]
JUAMI，非洲材料研究所的联合体：在大陆之间建立材料科学研究合作和能力
Simon J L Billinge
Simon J L Billinge
JUAMI, the joint undertaking for an African materials institute, is a project to build collaborations and materials research capabilities between PhD researchers in Africa, the United States, and the world. Focusing on research-active unive...
Ernesto Mesto,Coco K Y A Okio,Maria Alejandra Lemus et al.
Ernesto Mesto et al.
The synthesis and crystallographic analysis of the title compound, C9H9N3O2S, are reported. The compound crystallizes in the monoclinic space group P21/c, revealing characteristic bond lengths and angles typical of thio-semicarbazone groups...
Hanna Kaspiaruk,Lilianna Chęcińska
Hanna Kaspiaruk
The crystal structure of the new triclinic polymorph of miconazole {MIC; C18H14Cl4N2O; systematic name: (RS)-1-[2-(2,4-di-chloro-benz-yloxy)-2-(2,4-di-chloro-phen-yl)eth-yl]-1H-imidazole} is reported and compared with the monoclinic form of...
Crystal structures and Hirshfeld surface analyses of methyl 4-{2,2-di-chloro-1-[(E)-phenyl-diazen-yl]eth-enyl}benzoate, methyl 4-{2,2-di-chloro-1-[(E)-(4-methyl-phen-yl)diazen-yl]ethen-yl}benzoate and methyl 4-{2,2-di-chloro-1-[(E)-(3,4-di-methyl-phen-yl)diazen-yl]ethen-yl}benzoate [0.03%]
甲基4-{2,2-二氯-1-[（E）-苯基-叠氮基]乙烯基}苯甲酸酯，甲基4-{2,2-二氯-1-[（E）-（4-甲基苯基）叠氮基]乙烯基}苯甲酸酯和甲基4-{2,2-二氯-1-[（E）-（3,4-二甲基苯基）叠氮基]乙烯基}苯甲酸酯的晶体结构及Hirshfeld表面分析
Namiq Q Shikhaliyev,Shafiga A İbrahimova,Gulnar T Atakishiyeva et al.
Namiq Q Shikhaliyev et al.
The crystal structures and Hirshfeld surface analyses of three similar azo compounds are reported. Methyl 4-{2,2-di-chloro-1-[(E)-phenyl-diazen-yl]ethen-yl}benzoate, C16H12Cl2N2O2, (I), and methyl 4-{2,2-di-chloro-1-[(E)-(4-methyl-phen-yl)d...
Crystal structure and characterization of a new lanthanide coordination polymer, [Pr2(pydc)(phth)2(H2O)3]·H2O [0.03%]
新的稀土配合物聚合物[Pr2(pydc)(phth)2(H2O)3]·H2O的晶体结构和表征
Bunlawee Yotnoi,Apinpus Rujiwatra
Bunlawee Yotnoi
A new lanthanide coordination polymer, poly[[tri-aqua-bis-(μ4-phthalato)(μ3-pyridine-2,5-di-carboxyl-ato)dipraseodymium] monohydrate], {[Pr2(C7H3NO4)2(C8H4O4)(H2O)3]·H2O}n or {[Pr2(phth)2(pydc)(H2O)3]·H2O}n, (pydc2- = pyridine-2,5-di-ca...
Synthesis, crystal structure and Hirshfeld surface analysis of sodium bis-(malonato)borate monohydrate [0.03%]
钠双(丙二酸盐)硼酸盐水合物的合成、晶体结构及Hirshfeld表面分析
Ramalingam Selvi,Govindharajan Gokila,Aravazhi Amalan Thiruvalluvar et al.
Ramalingam Selvi et al.
In the title salt, poly[aqua-[μ4-bis-(malonato)borato]sodium], {[Na(C6H4BO8)]·H2O}n or Na+·[B(C3H2O4)2]-·H2O, the sodium cation exhibits fivefold coordination by four carbonyl O atoms of the bis-(malonato)borate anions and a water O ato...
(S)-(+)-1-(4-Bromo-phen-yl)- N-[(4-methoxyphen-yl)methyl-idene]ethyl-amine and bis-{(S)-(+)-1-(4-bromo-phen-yl)- N-[(4-methoxyphen-yl)methyl-idene]ethyl-amine-κ N}di-chlorido-palladium(II) [0.03%]
(S)-(+)-1-(4-溴苯基)-N-[(4-甲氧基苯基)亚甲基]乙胺和双-{(S)-(+)-1-(4-溴苯基)-N-[(4-甲氧基苯基)亚甲基]乙胺-κ N}二氯化钯(II)
Bertin Anzaldo,Gloria E Moreno Morales,Claudia P Villamizar C et al.
Bertin Anzaldo et al.
The (S)-(+)-1-(4-bromo-phen-yl)-N-[(4-methoxyphen-yl)methyl-idene]ethyl-amine ligand, C16H16BrNO, (I), was synthesized through the reaction of 4-meth-oxy-anisaldehyde with (S)-(-)-1-(4-bromo-phen-yl)ethyl-amine. It crystallizes in the ortho...
Synthesis, structure and Hirshfeld surface analysis of 2-oxo-2 H-chromen-6-yl 4- tert-butyl-benzoate: work carried out as part of the AFRAMED project [0.03%]
2-氧代-2H-色烯-6-基 4-叔丁基苯甲酸酯的合成、结构及希施菲尔德表面分析：作为AFRAMED项目的一部分所开展的工作
Patrice Kenfack Tsobnang,Eric Ziki,Soso Siaka et al.
Patrice Kenfack Tsobnang et al.
In the title compound, C20H18O4, the dihedral angle between the 2H-chromen-2-one ring system and the phenyl ring is 89.12 (5)°. In the crystal, the mol-ecules are connected through C-H⋯O hydrogen bonds to generate [010] double chains that...