Synthesis and crystal structures of bis-[1-oxopyridin-2-olato(1-)]bis-(penta-fluoro-phen-yl)silicon(IV)-tetra-hydro-furan-pentane (2/1/1), bis-[1-oxopyridin-2-olato(1-)]bis-(p-tol-yl)silicon(IV), and dimesitylbis[1-oxopyridin-2-olato(1-)]silicon(IV) [0.03%]
双-[1-氧代吡啶-2-醇盐(1-)]双-(五氟苯基)硅(IV)-四氢呋喃-戊烷 (2/1/1), 双-[1-氧代吡啶-2-醇盐(1-)]双-(对甲苯基)硅(IV), 和二甲基异丙基双[1-氧代吡啶-2-醇盐(1-)]硅(IV)的合成与晶体结构研究
Bradley M Kraft,William W Brennessel,Jordan W Andrews et al.
Bradley M Kraft et al.
The neutral organosilicon(IV) complex, (C6F5)2Si(OPO)2 (OPO = 1-oxopyridin-2-one, C5H4NO2), was synthesized from (C6F5)2Si(OCH3)2 and 2 equiv. of 1-hy-droxy-pyridin-2-one in tetra-hydro-furan (THF). Single crystals grown from the diffusion ...
Crystal structures of sulfonamide protected bicyclic guanidines: (S)-8-{[(tert-butyl-dimethyl-sil-yl)-oxy]meth-yl}-1-[(2,2,4,6,7-penta-methyl-2,3-di-hydro-benzo-furan-5-yl)sulfon-yl]-1,3,4,6,7,8-hexa-hydro-2 H-pyrimido[1,2- a]pyrimidin-1-ium tri-fluoro-methane-sulfonate and (S)-8-(iodo-meth-yl)-1-tosyl-1,3,4,6,7,8-hexa-hydro-2 H-pyrimido[1,2- a]pyrimidi [0.03%]
磺胺保护的双环胍的晶体结构：(S)-8-{[(叔丁基二甲基硅-基)氧]甲-基}-1-[(2,2,4,6,7-五甲基-2,3-二氢苯并呋喃-5-亚基]磺酰]-1,3,4,6,7,8-六氢-2 H-吡啶并[1,2- a]嘧啶
Jamal M H Alaboosh,Steven P Hill,Benson M Kariuki et al.
Jamal M H Alaboosh et al.
Two compounds, (S)-8-{[(tert-butyl-dimethyl-sil-yl)-oxy]meth-yl}-1-[(2,2,4,6,7-penta-methyl-2,3-di-hydro-benzo-furan-5-yl)sulfon-yl]-1,3,4,6,7,8-hexa-hydro-2H-pyrimido[1,2-a]pyrimidin-1-ium tri-fluoro-methane-sulfonate, C27H46N3O4SSi+·CF3O...
Florian Meurer,Jakob Möbs,Melanie Nentwich et al.
Florian Meurer et al.
Since its founding in 2013, the Young Crystallographers (YC) have become one of the most active working groups not only within their parent organization, the German Crystallographic Society (DGK), but also among other young crystallographer...
Crystal structure and Hirshfeld surface analysis of 3-phenyl-1-{3-[(3-phenyl-quinoxalin-2-yl)-oxy]prop-yl}-1,2-di-hydro-quinoxalin-2-one [0.03%]
3-[3-(3-苯基喹唑啉-2-基氧)丙基]-3-苯基-1,2-二氢喹唑啉-2-酮的晶体结构及其 Hirshfeld 表面分析
Nadeem Abad,Joel T Mague,Abdulsalam Alsubari et al.
Nadeem Abad et al.
In the title compound, C31H24N4O2, the quinoxaline units are distinctly non-planar and twisted end-to-end. In the crystal, C-H⋯O and C-H⋯N hydrogen bonds link the mol-ecules into chains extending along the a-axis direction. The chains are...
Crystal structure of 1-{4-[bis-(4-methyl-phen-yl)amino]-phen-yl}ethene-1,2,2-tricarbo-nitrile [0.03%]
1-{4-[双(4-甲基苯基)氨基]苯基}乙烯-1,2,2-三氰化物的晶体结构
Mamoun M Bader,Phuong-Truc Pham
Mamoun M Bader
The title compound, C25H18N4, crystallizes in the centrosymmetric ortho-rhom-bic space group Pbca, with eight mol-ecules in the unit cell. The main feature noticeable in the structure is the impact of the tri-cyano-vinyl (TCV) group in forc...
Crystal structure and Hirshfeld surface analysis of (Z)- N-{chloro-[(4-ferrocenylphen-yl)imino]-meth-yl}-4-ferrocenylaniline N, N-di-methyl-formamide monosolvate [0.03%]
(Z)-N-{氯-[-(4-亚铁氰基苯基)亚氨基]甲基}-4-亚铁氰基苯胺N，N-二甲基甲酰胺单溶剂的晶体结构和 Hirshfeld 表面分析
Riham Sghyar,Abdeslem Bentama,Amal Haoudi et al.
Riham Sghyar et al.
The title mol-ecule, [Fe2(C5H5)2(C23H17ClN2)]·C3H7NO, is twisted end to end and the central N/C/N unit is disordered. In the crystal, several C-H⋯π(ring) inter-actions lead to the formation of layers, which are connected by further C-H⋯...
Crystal structure of 4-(benzo[ d]thia-zol-2-yl)-1,2-dimethyl-1 H-pyrazol-3(2 H)-one [0.03%]
4-(苯并[d]噻唑-2-基)-1,2-二甲基-1H-吡唑-3(2H)-酮的晶体结构
Heba A Elboshi,Rasha A Azzam,Galal H Elgemeie et al.
Heba A Elboshi et al.
In the title compound, C12H11N3OS, the inter-planar angle between the pyrazole and benzo-thia-zole rings is 3.31 (7)°. In the three-dimensional mol-ecular packing, the carbonyl oxygen acts as acceptor to four C-H donors (with one H⋯O as s...
Crystal structure and characterization of a new one-dimensional copper(II) coordination polymer containing a 4-amino-benzoic acid ligand [0.03%]
含有4-氨基苯甲酸配体的一种新的二维铜（II）配位聚合物的晶体结构与表征
Alisha Gogia,Egor M Novikov,Ilia A Guzei et al.
Alisha Gogia et al.
A CuII coordination polymer, catena-poly[[[aqua-copper(II)]-bis-(μ-4-amino-benz-o-ato)-κ2 N:O;κ2 O:N] monohydrate], {[Cu(pABA)2(H2O)]·H2O}n (pABA = p-amino-benzoate, C7H4NO2 -), was synthesized and characterized. It exhibits a one-dimen...
Crystal structure, Hirshfeld surface analysis and DFT study of N-(2-nitro-phen-yl)male-imide [0.03%]
N-(2-硝基苯基)-马来酰亚胺的晶体结构、Hirshfeld表面分析及DFT研究
Maribel Montoya-Garcia,Héctor Cortes-Hernandez,Richard D&#x;Vries et al.
Maribel Montoya-Garcia et al.
The title compound [systematic name: 1-(2-nitro-phen-yl)pyrrole-2,5-dione], C10H6N2O4, crystallizes in the monoclinic system (space group P21/n) with two mol-ecules in the asymmetric unit, which are linked by C-H⋯O hydrogen bonds. Hirshfel...
Crystal structures of five gold(I) complexes with methyl-piperidine ligands [0.03%]
具有甲基哌啶配体的五个金(I)配合物的晶体结构
Cindy Döring,Peter G Jones
Cindy Döring
In bis-(4-methyl-piperidine-κN)gold(I) chloride, [Au(C6H13N)2]Cl (1), the methyl groups are, as expected, equatorial at the piperidine ring, but the Au atom is axial; this is the case for all five structures reported here, as is the expect...