Synthesis, characterization, and crystal structure of 2-(2-azido-phen-yl)-3-oxo-3 H-indole 1-oxide [0.03%]
2-(2-叠氮苯基)-3-氧代-3H-吲哚氧化物的合成、表征及晶体结构分析
Pawan Dhote,Srinu Tothadi,Chepuri V Ramana
Pawan Dhote
An attempt to explore the reactivity of the nitro group in the presence of gold catalysis in comparison to the azide group yielded intriguing results. Surprisingly, only the nitro group exhibited reactivity, ultimately giving rise to the fo...
Crystal structure of di-ethyl-ammonium dioxido{ Z)- N-[(pyri-din-2-yl)car-bon-yl-azan-idyl]pyri-dine-2-car-box-imid-ato}vana-date(1-) monohydrate [0.03%]
二乙基铵{(Z)-N-(吡啶-2-基碳酰亚氨基)吡啶-2-羧脒基}矾酸(1-)单水合物的晶体结构
Bipul Mondal
Bipul Mondal
The title compound, (C4H12N)[V(C12H8N4O2)O2]·H2O, was synthesized via aerial oxidation on refluxing picolinohydrazide with ethyl picolinate followed by addition of VIVO(acac)2 and di-ethyl-amine in methanol. It crystallizes in the triclini...
Crystal structure of the sodium salt of mesotrione: a triketone herbicide [0.03%]
mesotrione（一种三酮类除草剂）钠盐的晶体结构研究
Olha Bereziuk,Kateryna Gubina,Viktor Trush et al.
Olha Bereziuk et al.
The crystal structure of the sodium salt of mesotrione, namely, catena-poly[[sodium-μ3-2-[(4-methane-sulfonyl-2-nitro-phen-yl)carbon-yl]-3-oxo-cyclo-hex-1-en-1-olato] ethanol monosolvate], {[Na(C14H12NO7S)]C2H5OH}n, is described. The X-ray...
Crystal structure of tetra-kis-(μ-2-hy-droxy-3,5-di-isoprop-yl-benzoato)bis-[(dimethyl sulfoxide)copper(II)] [0.03%]
四(μ-2-羟基-3,5-二异丙基苯甲酸)双[(二甲亚砜)铜(II)]的晶体结构
Daniel G Shlian,Rachael H Summers,Katelyn Martinez et al.
Daniel G Shlian et al.
Metal complexes of 3,5-diiso-propyl-salicylate are reported to have anti-inflammatory and anti-convulsant activities. The title binuclear copper complex, [Cu2(C13H17O3)4(C2H6OS)2] or [Cu(II)2(3,5-DIPS)4(DMSO)2], contains two five-coordinate...
Structural characterization of a new samarium-sodium heterometallic coordination polymer [0.03%]
一个新的钐钠杂金属配位聚合物的结构表征
Ashley M Hastings,Ashley Williams,Robert G Surbella Iii et al.
Ashley M Hastings et al.
Lanthanide-containing materials are of inter-est in the field of crystal engin-eering because of their unique properties and distinct structure types. In this context, a new samarium-sodium heterometallic coordination polymer, poly[tetra-ki...
Crystal structure and Hirshfeld surface analysis of 4-oxo-3-phenyl-2-sulfanyl-idene-5-(thio-phen-2-yl)-3,4,7,8,9,10-hexa-hydro-2 H-pyrido[1,6- a:2,3- d']di-pyrimidine-6-carbo-nitrile [0.03%]
4-氧代-3-苯基-2-硫代烯基-5-(噻吩-2-基)-3,4,7,8,9,10-六氢-2H-吡啶并[1,6-a:2,3-d']双嘧啶-6-腈的晶体结构和希施菲尔德表面分析
Farid N Naghiyev,Victor N Khrustalev,Mehmet Akkurt et al.
Farid N Naghiyev et al.
In the title compound, C21H15N5OS2, mol-ecular pairs are linked by N-H⋯N hydrogen bonds along the c-axis direction and C-H⋯S and C-H⋯O hydrogen bonds along the b-axis direction, with R 2 2(12) and R 2 2(16) motifs, respectively, thus for...
Syntheses, characterizations, crystal structures and Hirshfeld surface analyses of methyl 4-[4-(di-fluorometh-oxy)phen-yl]-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexa-hydro-quinoline-3-carboxyl-ate, isopropyl 4-[4-(di-fluoro-meth-oxy)phen-yl]-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexa-hydro-quinoline-3-carboxyl-ate and tert-butyl 4-[4-(di-fluoro-meth-oxy)phen-yl [0.03%]
甲基4-[4-(二氟甲氧基)苯基]-2,7,7-三甲基-5-氧代-1,4,5,6,7,8-六氢喹啉-3-羧酸酯、异丙基4-[4-(二氟甲氧基)苯基]-2,6,6-三甲基-5-氧代-1,4,5,6,7,8-六氢喹啉-3-羧酸酯和特丁基4-[4-(二氟甲氧基)苯基]的合成、表征、晶体结构及希施菲尔德表面分析
Sema Öztürk Yıldırım,Mehmet Akkurt,Ezgi Pehlivanlar et al.
Sema Öztürk Yıldırım et al.
The crystal structures and Hirshfeld surface analyses of three similar compounds are reported. Methyl 4-[4-(di-fluoro-meth-oxy)phen-yl]-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexa-hydro-quinoline-3-carboxyl-ate, (C21H23F2NO4), (I), crystallizes ...
Omadacycline dihydrate, C29H40N4O7·2H2O, from X-ray powder diffraction data [0.03%]
来自X射线粉末衍射数据的奥马扎西环素二水合物，C29H40N4O7·2H2O
James A Kaduk,Nicholas C Boaz,Stacy Gates-Rector et al.
James A Kaduk et al.
The crystal structure of the title compound {systematic name: (4S,4aS,5aR,12aR)-4,7-bis-(di-methyl-amino)-9-[(2,2-di-methyl-propyl-amino)-meth-yl]-1,10,11,12a-tetra-hydroxy-3,12-dioxo-4a,5,5a,6-tetra-hydro-4H-tetra-cene-2-carb-oxamide dihyd...
[4-(2-Aminoethyl)morpholine-κ2N, N']di-bromidocadmium(II): synthesis, crystal structure and Hirshfeld surface analysis [0.03%]
4-(2-氨基乙基)吗啉-κ2N, N'二溴化镉(II): 合成，晶体结构和Hirshfeld表面分析
B Chidambaranathan,S Sivaraj,P Vijayamathubalan et al.
B Chidambaranathan et al.
The title compound, [CdBr2(C6H14N2O)], was synthesized upon complexation of 4-(2-aminoethyl)morpholine and cadmium(II) bromide tetra-hydrate at 303 K. It crystallizes as a centrosymmetric dimer, with one cadmium atom, two bromine atoms and ...
Crystal structure of the tetra-ethyl-ammonium salt of the non-steroidal anti-inflammatory drug nimesulide (polymorph II) [0.03%]
非甾体抗炎药Nimesulide的四乙基铵盐的晶体结构（多晶型II）
Małgorzata Rybczyńska,Artur Sikorski
Małgorzata Rybczyńska
The crystal structure of the tetra-ethyl-ammonium salt of the non-steroidal anti-inflammatory drug nimesulide (polymorph II) (systematic name: tetra-ethyl-ammonium N-methane-sulfonyl-4-nitro-2-phen-oxy-anilinide), C8H20N+·C13H11N2O5S-, was...