Structure of the five-coordinate CoII complex (1 H-imidazole){tris-[(1-benzyl-triazol-4-yl-κ N3)meth-yl]amine-κ N}cobalt(II) bis-(tetra-fluoro-borate) [0.03%]
五配位的CoII配合物（1H-咪唑）{三[（1-苄基-1,2,4-三氮唑-4-基-κN3）甲基]胺-κN}氯化钴双(四氟硼酸盐)的结构
Vipul Batra,Garrett C Reed,David L Tierney
Vipul Batra
The title compound, [Co(C3H4N2)(C30H30N10)](BF4)2, is a five-coordinate CoII complex based on the neutral ligands tris-[(1-benzyl-triazol-4-yl)meth-yl]amine (tbta) and imidazole. It exhibits a distorted trigonal bipyramidal geometry in whic...
Crystal structure, Hirshfeld surface analysis, calculations of crystal voids, inter-action energy and energy frameworks as well as density functional theory (DFT) calculations of 3-[2-(morpholin-4-yl)eth-yl]-5,5-di-phenyl-imidazolidine-2,4-dione [0.03%]
3-[2-（吗啉-4-基）乙基]-5,5-二苯基-1,3-二氧杂螺[4.4]壬-2-酮的晶体结构、 Hirshfeld 表面分析及空穴、相互作用能和能量体系的计算以及基于密度泛函理论（DFT）的计算
Houda Lamssane,Amal Haoudi,Badr Eddine Kartah et al.
Houda Lamssane et al.
In the title mol-ecule, C21H23N3O3, the imidazolidine ring slightly deviates from planarity and the morpholine ring exhibits the chair conformation. In the crystal, N-H⋯O and C-H⋯O hydrogen bonds form helical chains of mol-ecules extendin...
Crystal structure of tetra-phenyl phosphate tetra-kis-[dimethyl (2,2,2-tri-chloro-acet-yl)phos-pho-ramidato]lutetium(III), PPh4[Lu L4] [0.03%]
四苯基磷酸四[{双（2,2,2-三氯乙酰）亚氨基}二甲基]镥(III)，PPh4[LuL4]的晶体结构
Mariia B Struhatska,Vladimir A Ovchynnikov,Nataliia S Kariaka et al.
Mariia B Struhatska et al.
A lutetium(III) complex based on the anion of the ligand dimethyl (2,2,2-tri-chloro-acet-yl)phospho-ramidate (HL) and tetra-phenylphosphonium, of composition PPh4[LuL 4] (L = CAPh = carbacyl-amido-phosphate), or (C24H20)[Lu(C4H6Cl3NO4P)4], ...
Synthesis, crystal structure and Hirshfeld surface analysis of 2-phenyl-3-(prop-2-yn-1-yl-oxy)quin-oxaline [0.03%]
2-苯基-3-(丙-2-烯-1-基氧)喹 oxaline 的合成、晶体结构及 Hirshfeld 表面分析
Nadeem Abad,Joel T Mague,Abdulsalam Alsubari et al.
Nadeem Abad et al.
In the title compound, C17H12N2O, the quinoxaline moiety shows deviations of 0.0288 (7) to -0.0370 (7) Å from the mean plane (r.m.s. deviation of fitted atoms = 0.0223 Å). In the crystal, corrugated layers two mol-ecules thick are formed ...
Crystal structure and Hirshfeld surface analysis of ethyl 2-(7-chloro-3-methyl-2-oxo-1,2-di-hydro-quinoxalin-1-yl)acetate [0.03%]
乙基2-（7-氯-3-甲基-2-氧代-1,2-二氢基喹唑啉-1-基）乙酸酯的晶体结构及Hirshfeld面分析
Nour El Hoda Mustaphi,Fatima Ezzahra Aboutofil,Lamyae El Houssni et al.
Nour El Hoda Mustaphi et al.
The quinoxaline moiety in the title mol-ecule, C13H13ClN2O3, is almost planar (r.m.s. deviation of the fitted atoms = 0.033 Å). In the crystal, C-H⋯O hydrogen bonds plus slipped π-stacking and C-H⋯π(ring) inter-actions generate chains ...
Synthesis and crystal structure of tetra-methyl (E)-4,4'-(ethene-1,2-di-yl)bis-(5-nitro-benzene-1,2-di-carboxyl-ate) [0.03%]
(E)-4,4'-（乙烷-1,2-二基）双（5-硝基苯并[1,2-]二甲酸四甲酯）的合成和晶体结构
Artjom Businski,Thuy C Ta,Niklas Gindullis et al.
Artjom Businski et al.
The title compound, C22H18N2O12, was obtained as a by-product during the planned synthesis of 1,2-bis-(2-nitro-4,5-dimethyl phthalate)ethane by oxidative dimerization starting from dimethyl-4-methyl-5-nitro phthalate. To identify this compo...
CoII-catalysed synthesis of N-(4-meth-oxy-phen-yl)-5-(pyridin-4-yl)-1,3,4-oxa-diazol-2-amine hemi-hydro-chloride monohydrate [0.03%]
N-(4-甲氧基苯基)-5-(吡啶-4-基)-1,3,4-噁二氮杂卓-2-胺半盐酸单 hydrate 的 CoII 催化合成
Ram N Gautam,Sankatha P Sonkar,Shailendra Yadav et al.
Ram N Gautam et al.
The title compound, C14H12N4O2·0.5HCl·H2O or H(C14H12N4O2)2 +·Cl-·2H2O, arose from the unexpected cyclization of isonicotinoyl-N-phenyl hydrazine carbo-thio-amide catalysed by cobalt(II) acetate. The organic mol-ecule is almost planar a...
Synthesis and crystal structure of N-phenyl-2-(phenyl-sulfan-yl)acetamide [0.03%]
N-(苯基)-2-(苯硫基)乙酰胺的合成与晶体结构测定
Reham A Mohamed-Ezzat,Benson M Kariuki,Galal H Elgemeie
Reham A Mohamed-Ezzat
N-Phenyl-2-(phenyl-sulfan-yl)acetamide, C14H13NOS, was synthesized and structurally characterized. In the crystal, N-H⋯O hydrogen bonding leads to the formation of chains of mol-ecules along the [100] direction. The chains are linked by C-...
Crystal structures of ten phosphane chalcogenide complexes of gold(III) chloride and bromide [0.03%]
十种金(III)卤化物与磷烷硫属化合物的晶体结构
Daniel Upmann,Dirk Bockfeld,Peter G Jones et al.
Daniel Upmann et al.
The structures of ten phosphane chalcogenide complexes of gold(III) halides, with general formula R 1 3-n R 2 nPEAuX 3 (R 1 = t-butyl; R 2 = i-propyl; n = 0 to 3; E = S or Se; X = Cl or Br) are presented. The eight possible chlorido derivat...
The unanti-cipated oxidation of a tertiary amine in a tetra-cyclic glyoxal-cyclam condensate yielding zinc(II) coordinated to a sterically hindered amine oxide [0.03%]
关于四环型双环己酮- cyclam 缩合物中一个叔胺的不可预见氧化以及由此得到的一个锌(ii)与受空间位阻影响胺氧基配体相配合的研究
Daniel J Hubin,Blue M Cunningham,Timothy J Hubin et al.
Daniel J Hubin et al.
The complex, tri-chlorido-(1,4,11-tri-aza-8-azonia-tetra-cyclo-[6.6.2.04,16.011,15]hexa-decane 1-oxide-κO)zinc(II) monohydrate, [ZnCl3(C12H23N4O)]·H2O, (I), has monoclinic symmetry (space group P21/n) at 120 K. The zinc(II) center adopts ...