Crystal structure of (E)-4-{2-[4-(all-yloxy)phen-yl]diazen-yl}benzoic acid [0.03%]
(Ε)-4-(2-[4-(丙氧基)苯基]叠氮基)苯甲酸的晶体结构
Md Lutfor Rahman,Mashitah Mohd Yusoff,Jamil Ismail et al.
Md Lutfor Rahman et al.
The title compound, C16H14N2O3, has an E conformation about the azo-benzene [-N=N- = 1.2481 (16) Å] linkage. The benzene rings are almost coplanar [dihedral angle = 1.36 (7)°]. The O atoms of the carb-oxy-lic acid group are disordered ove...
Crystal structure of di-μ-chloro-acetato-hexa-kis-(di-methyl-formamide)-tetra-kis-(μ-N,2-dioxido-benzene-1-carboximidato)tetra-manganese(III)disodium dimethyl-formamide disolvate [0.03%]
二氯化六-(N,N-二甲基甲酰胺)四-(μ-2-氧代苯甲胲)四锰(III)二钠二水合物的晶体结构
Connor I Daly,Matthias Zeller,Curtis M Zaleski
Connor I Daly
The synthesis, crystal structure, and FT-IR data for the title compound, [Na2Mn4(C2H2ClO2)2(C7H4NO3)4(C3H7NO)6]·2C3H7NO or Na2(O2CCH2Cl)2[12-MCMn(III) N(shi)-4](DMF)6·2DMF, where MC is metallacrown, shi(3-) is salicyl-hydroximate, and DMF...
Erik Hennings,Horst Schmidt,Wolfgang Voigt
Erik Hennings
The title compounds, calcium perchlorate tetra-hydrate and calcium perchlorate hexa-hydrate, were crystallized at low temperatures according to the solid-liquid phase diagram. The structure of the tetra-hydrate consists of one Ca(2+) cation...
Unexpected formation and crystal structure of tetra-kis-(1H-pyrazole-κN (2))-palladium(II) dichloride [0.03%]
二氯化四(1H-吡唑-κN(2))合 palladium(II)的形成和晶体结构（英文）
Thomas Wagner,Nena Christiansen,Cristian G Hrib et al.
Thomas Wagner et al.
The title salt, [Pd(C3H4N2)4]Cl2, was obtained unexpectedly by the reaction of palladium(II) dichloride with equimolar amounts of 1-chloro-1-nitro-2,2,2-tris-(pyrazol-yl)ethane in methanol solution. The Pd(2+) cation is located on an invers...
Crystal structure of hexa-kis-(μ2-4-tert-but-oxy-4-oxobut-2-en-2-olato)trizinc [0.03%]
四叔丁氧基取代的三核锌配合物的晶体结构测定：一个三重互变异构异彩纷呈的例子
Olgerd O Shtokvish,Lyudmila I Koval,Vasyl I Pekhnyo
Olgerd O Shtokvish
The title complex, systematic name hexa-kis-(μ2-4-tert-but-oxy-4-oxobut-2-en-2-olato)-1:2κ(9) O (2),O (4):O (2);2:3κ(9) O (2),O (4):O (2)-trizinc, [Zn3(C8H13O3)6], syn-the-sized from tert-butyl aceto-acetate and di-ethyl-zinc, consists o...
Erik Hennings,Horst Schmidt,Wolfgang Voigt
Erik Hennings
The title compound, [SnCl4(H2O)2]·6H2O, was crystallized according to the solid-liquid phase diagram at lower temperatures. It is built-up of SnCl4(H2O)2 octa-hedral units (point group symmetry 2) and lattice water mol-ecules. An intricate...
Erik Hennings,Horst Schmidt,Wolfgang Voigt
Erik Hennings
Since the discovery of perchlorate salts on Mars and the known occurrence of ferric salts in the regolith, there is a distinct possibility that the title compound could form on the surface of Mars. [Fe(H2O)6](ClO4)3·3H2O was crystallized f...
Erik Hennings,Horst Schmidt,Martin Köhler et al.
Erik Hennings et al.
The title compound, [Sn(H2O)3](ClO4)2, was synthesized by the redox reaction of copper(II) perchlorate hexa-hydrate and metallic tin in perchloric acid. Both the trigonal-pyramidal [Sn(H2O)3](2+) cations and tetra-hedral perchlorate anions ...
Crystal structure of bis-(propane-1,3-diaminium) hexa-fluorido-aluminate di-aqua-tetra-fluorido-aluminate tetra-hydrate [0.03%]
双(propane-1,3-二铵)六氟合铝酸根二水四氟合铝酸盐四 hydrate晶体结构
Insaf Abdi,Khulood Al-Sadhan,Amor Ben Ali
Insaf Abdi
The title compound, (C3H12N2)2[AlF6][AlF4(H2O)2]·4H2O, was obtained by a solvothermal method in ethanol as solvent and with aluminium hydroxide, HF and 1,3-di-amino-propane as educts. The asymmetric unit contains a quarter each of two crys...
Vitaliia Fedyna,Roksolana Kozak,Roman Gladyshevskii
Vitaliia Fedyna
A single crystal of the title compound, the ternary silicide digadolinium trirhenium penta-silicide, Gd2Re3Si5, was isolated from an alloy of nominal composition Gd20Re30Si50 synthesized by arc melting and investigated by X-ray single-cryst...