From ball-milling to bead-milling technology: rapid optimization and scale-up of a one-pot Wittig olefination-Diels-Alder reaction sequence using an agitator bead mill
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Mechanochemical methods offer a sustainable alternative to traditional solution-based synthesis, yet their scalability beyond laboratory-scale ball mills remains a challenge and often requires lengthy re-optimization for larger scales. Herein, we report the ra... ...
