Scaling Azapeptide with N-Fmoc-Aza-Tripeptide from Resonant Acoustic Mixing of N-Fmoc-Amino Hydrazide and N-Succinimidyl Carbamate
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Sustainable and scalable solution-phase synthesis of aza-tripeptide building-blocks was achieved by using resonant acoustic mixing (RAM). Hydrazinolysis gave N-(Fmoc)amino hydrazide without Fmoc cleavage, diacylation, epimerization, and chromatographic purific... ...
