Pd(II)-Catalyzed Hydroxyl-acyloxylation of gem-Dimethyl Groups via Dual C(sp3)-H Activation
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Herein, we report a one-pot dual oxyfunctionalization reaction of ubiquitous gem-dimethyl groups using a single Pd(II)/Pd(IV) catalytic system, achieving both hydroxyl-acyloxylation and diacetoxylation by employing N-pyridine ylide as a directing group. This s... ...
