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Extensive de novo solid-state NMR assignments of the 33 kDa C-terminal domain of the Ure2 prion

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We present the de novo resonance assignments for the crystalline 33 kDa C-terminal domain of the Ure2 prion using an optimized set of five 3D solid-state NMR spectra. We obtained, using a single uniformly (13)C, (15)N labeled protein sample, sequential chemica... ...