Ab initio structure determination and Rietveld refinement of a high-temperature phase of zirconium hydrogen phosphate and a new polymorph of zirconium pyrophosphate from in situ temperature-resolved powder diffraction data
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The collected in situ temperature-resolved synchrotron powder data revealed that the transformation of the recently reported three-dimensional tau-Zr(HPO4)2 to cubic ZrP2O7 goes through two intermediate phases. The first intermediate phase, rho-Zr(HPO4)2, is f... ...
